Thank you for the suggestions. Yes, some of what I'm doing does not require the ISTD but I leave it in the analysis method b/c of needing it in some of the work. I haven't had a chance to work on this in a couple of weeks, but will definitely keep it…
Hello Adrsto ,
I apologize for the delayed repsonse.
It is not possible to use the NIST algorithm itself within Unknowns Analysis. As you mentioned, you can adjust the forward and reverse settings and enable the Adjust Score option, which from the…
Hello Lstephan ,
I apologize for the delayed response.
Errors of this type generally point to an issue with a preferences file. The first thing to try is clearing these using the Restore User Settings tool found in the Quant Tools group in the start…
Hello AJohnson13 ,
This is a known issue if Acquisition has been pinned to the Windows Taskbar and run from there in MassHunter Acq Version 11.x and later. This is due to the OpenLab integration and the need to launch through Control Panel to include…
Please give more information. TSU - is that Thermal Screening Unit? You say under varying pressures...from zero to how many PSI/Bar? Will you need to use a vacuum to get the sample? Will this be analytes in air or something else? Decomposition of what…
Did the EM get replaced March 15? Or a source cleaning? The EMV went down 883V.
The Ent Lens (Entrance Lens) those jumps from 16 to 63,32,47.5 .. and the Ion Focus going from 80's to 40's... make me jumpy. Something was changing. When were source cleanings…
The ID testing process in the pharmaceutical industry often exposes warehouse staff to hazardous materials. This new technical note shows how pharmaceutical manufacturing QA/QC organizations can use the Agilent Vaya Raman system to check raw materials…
Hello community,
I have the following error (attached images) when start either offline or online mode. As you can see, the module control panel also dissappear. I have checked all the conections between PC and all modules and the error window continue…
This Information Applies To: HES ion source in 5977B/C GC/MSD, 7010 triple quadrupole GC/MS systems
Issue
The filaments are replaced as part of routine maintenance, or when they break (zero output current).
Items Required
Gloves, nylon,...
This Information Applies To: Agilent 5977A/B/C GC/MSD
Issue
The Electron Multiplier Horn must be replaced when it is contaminated or the EMV value reaches 3000 V with a clean ion source.
Items Required
Electron multiplier horn (5977B/C:...
This Information Applies To: Agilent 5973/ 5975/5977 GC/MSD with rotary vane foreline pump
Issue:
The oil mist filter is recommended to be replaced annually. If the color of the filter has changed or there is smell from the filter, the oil mist...
This Information Applies To: Agilent EI Source
Issue:
During normal operation of the GC/MS, the EI SST/Inert ion source will need to be disassembled to proceed with abrasive ion source cleaning and / or routine replacement of consumable parts (filaments...
This Information Applies To: Agilent G7129A/B/C Vialsampler
Issue:
Replacing the needle and needle seat of the Vialsampler is required when:
The needle is visibly damaged.
Leaks or blockages in the vialsampler are observed, especially between...
This Information Applies To: Agilent G1311A/B/C, G7111A/B, Quaternary Pumps, and G1310A/B, G7110B Isocratic Pumps, G1312A/B/C, G7112B Binary Pumps
Issue:
How to diagnose no flow or no pressure issues on binary, quaternary, or isocratic pumps.
...
This Information Applies To: Agilent UV and RID detectors
Issue
A clogged flow cell causes high backpressure. The clog can be removed by flushing the system with solvents at high pressure. If you suspect a clog or experience high backpressure due...
This Information Applies To: Agilent G1312X and G7112X binary pumps.
Issue:
A blockage before the pressure sensor, e.g. in a pump head, will not give a high pressure or overpressure system error. Instead, the pump may show one of various error messages...
This Information Applies To: Agilent 1100, 1200, 1260 LC Pumps.
Issue:
The following procedure allows the cleaning of residue from the pump's check valves, often caused by polymerization of aged acetonitrile or salt-based solutions that may prevent...
This Information Applies To: Agilent LC Systems
Issue
After analyzing dirty or concentrated samples, some sample compounds may retain in the column and other parts of the HPLC system. If the column re-equilibration after each run is not enough to...