Hi, Here's a screenshot of the system suit, there is no blank subtraction The analyst said he has used the same processing method for a different run with no issues the only difference being that for those runs the MS setting was the same time as the…
The basic tools I would recommend to have for GC maintenance:
Ceramic column cutter
1/4" wrench (column nuts)
7/16" wrench (gas fittings at back of GC)
1/2" wrench (replace gold seal on S/SL inlet)
Torx 20 driver (removing FID collector assembly…
When you say that there are no signs of a leak, have you run a pump leak rate test using Agilent Lab Advisor? If not, I would suggest testing this. If you're unlucky enough for your peak to elute just at the point when the outlet ball valve fails to close…
Agilent GC 7890A, FID, Split Liner. I'm setting up the column to do Hexane injection testing. It was set up this way previously but the program had been deleted and the column removed before I started here. Front Detector/Column which is below baseline…
Hello and Help!
My GC-FID's inlet pressure stays at 0.7 psi and does not reach the setpoint of 10 psi. Makeup gas reaches the 25 psi setting. Liner and septa are fine. I unscrewed the inlet column nut and placed my finger at the bottom of the inlet…
Hello,
My laboratory runs a multilevel calibration with internal standards on a headspace-GC-FID. Our sequence is set up to replace each level of the curve after each calibrator is analyzed and then calculate the concentration of the analyte with the…
I'm going to be calibrating for ethanol on my HS-GC-FID 6890, but I'm having discrepancies between two standards. The standard that I will be calibrating with (Restek's Residual Solvents #1 34105) is 3000ug/mL in N,N-Dimethylacetamide. I'm verifying the…
Hi Dr. Know
Here is some of the information you have requested. Please let me know if you need any further info.
How is your system configured? FID detector using helium as carrier gas, nitrogen as makeup gas.
Which phases are the two columns…
Hi
I am pretty new to GCMS, so may need extra details on how to do things you suggest
I attached a picture of the set up of our gc system, so I can explain better. We recently installed a guard column using 30 cm piece of FS Deactivated 0.250 mm(Agilent…
First of all, thank you for posting publicly, I had not noticed this interface feature of MassHunter Quant, it looks very useful.
Were you able to get it working in 11.1?
If you're allowed to share your "IScriptable" folder, I would be very interested…
This Information Applies To: Agilent ICP Expert software.
Issue
The software version is often asked and is a valuable information: to see if any updates are needed, if certain options are available etc.
Steps to Follow
Launch ICP Expert...
This Information Applies To: Agilent OpenLab CDS
Issue
This article provides step-by-step instructions to calculate peak-to-valley ratio in OpenLab CDS.
Background
The peak-to-valley ratio is calculated to indicate the quality of peak separation...
This Information Applies To: Agilent 6500 Series Q-TOF LC/MS systems, MassHunter Workstation 10.1 or below and MassHunter Workstation 11.0 .
Issue
Fully reset the Q-TOF LC/MS system via a power cycle without venting. For users who experience slow...
This Information Applies To: Agilent 5200/5300/5400 Fragment Analyzer, Femto Pulse, ZAG DNA Analyzer, and Oligo Pro II systems
Issue
The volume of sample used by Agilent parallel capillary electrophoresis systems during a run.
Resolution
The...
This Information Applies To: Agilent 2100 Expert software, 2100 Expert Security Pack, 2100 Bioanalyzer
Issue
When opening the 2100 Expert software and using the Security Pack, the error message " Start of launcher application failed - The requested...
This Information Applies To: Agilent 6890, 6850, 7890, 8890, 8860, Intuvo 9000 GC systems.
Issue
The exchange of the ignitor in a Flame Photometric Detector (FPD) may be required in the following scenarios:
Preventive or periodic maintenance...
This Information Applies To: Agilent 1290 Infinity Quaternary Pump G4204A, 1290 Infinity II Flexible Pumps G7104A/C, and G7131A/C.
Issue
If the flexible/quaternary pump does not generate flow or build up pressure, it could be due to a stuck inlet...
This Information Applies To: Agilent 5200, 5300 and 5400 Fragment Analyzer systems
Issue
Separation times for the Fragment Analyzer for each array format and kit.
Resolution
Caution : The times in this article are the length of time...
This Information Applies To: Agilent 5200/5300/5400 Fragment Analyzer, Femto Pulse, ZAG DNA Analyzer, Oligo Pro II, ProteoAnalyzer systems
Issue
Guidance for installing the Agilent parallel capillary electrophoresis instrument controller and/or...
This Information Applies To: OpenLab CDS (version 2.x) system
Issue:
This article explains how to export OpenLab CDS 2.x data as Archived file.
For copying OpenLab CDS 2.x data to another Projects or another OpenLab CDS systems, you can use data...