Good day . i have another issue to my 8890. after replacing the fused silica in transfer line. tha air flow in FID is suddenly shutting down. then i try the detector diagnostic in the system it said test failed and need to replace the jet.
after replacing…
Hello,
this look like your plasma is not align with the cones. For the EM to failed it's difficult. You have to check for noise when it's doing it and if the counts are low when it's using mass 80. You can try to tune EM with mass 37 if you know where…
Try to ignite the plasma, without fixing the shield plate. Due to poor quality of argon gas or leak on gas line, reflected power will be above the limit and prevent the plasma sustain. Sometimes, the plasma sensor fiber optics tip is damaged, needs to…
Hello,
I am currently developing a residual solvent analysis method by Gas chromatography equipped with a flame ionization detector. My sample is an API with a phosphate salt attached. One of the residual solvents of interest is triethylamine. When…
8/7/19
Hello,
I have had a fair amount of success with posted questions in this forum, so here is another one. I am interested in knowing more about whether the flame ionization detector I have equipped on my HP/Agilent 6890 GC is the correct detector…
We have a lot of 1260s and 1290s in our lab, and as part of our sustainability initiatives are looking for ways to reduce our energy usage. Currently, all the instruments are left on (standby), and most of them also have the lamps on when not in use.…
When I need information about detectors I use the following books:
Raymond P. W. Scott "Chromatographic Detectors - Design, Function, and Operation", Chromatographic Science Series Volume 73, Marcel Dekker, New York (1996). ISBN 0-8247-9779-5.
Raymond…
Hi Guys,
I have a GC that does not seperate natural gas(maily C1 and C2 with small traces of C3+), it comes as almost one peak, and for condensate (C3+) it seperates C6+, and does not seperate C3÷C5,
I Have,
1: Readjusted the split ratio Many Many…
Hello Inês,
Typically we use the Performance report as a general health report of the instrument. Changing plasma parameters may cause the test to fail, unless you correct the limits. Moving the sample depth will decrease sensitivity and can increase…
Hello
I'm trying to setup report to have values in column "PASS/FAIL" green or red depends on result.
Can I do it as conditional formatting for column "PASS/FAIL" to mark FAIL as red based on text?
This column "PASS/FAIL" is custom field and…
This Information Applies To: 4150 TapeStation, 4200 TapeStation
Issue
How to deal with a TapeStation Electrode Cartridge change is due warning message.
Background
The Agilent TapeStation controller software will notify users to replace the...
This Information Applies To: Agilent OpenLab CDS
Issue
Sometimes the integration result is not ideal for all injections. This article outlines the step-by-step instruction to manually integrate peaks.
Background
There are 2 ways to integrate...
This Information Applies To: Agilent OpenLab CDS , Agilent OpenLab ChemStation
Issue
Calculation of Area percent or Height percent for uncalibrated compounds in OpenLab software. If all components respond equally in the detector, then Area% and...
This Information Applies To: Agilent ICP-MS (7700/7800/7850/7900/8800/8900)
Issue
How to power off the Agilent ICP-MS Foreline Pump to perform maintenance, or when fully powering off the Agilent ICP-MS System.
Background
The ICP-MS MassHunter...
This Information Applies To: Agilent ICP-MS (7500,7700,8800)
Issue
How to check the E2M18 or E2M18F foreline pump to determine if the pump needs maintenance?
Background
The oil cleanliness and oil level in the E2M18 or E2M18F foreline pump...
This Information Applies To: Agilent ICP-MS (7700/7800/8800)
Issue
How to replace the foreline pump oil in the DS 402.
Background
The DS 402 oil should be replaced at least every 3 months or when the oil color indicates it needs to be changed...
This Information Applies To: Agilent 8890/8860 GC Systems
Issue
How to delete data that is stored on the GC instrument.
Steps to follow
Caution : Before deleting data from your GC, Agilent recommends extraction of data as a backup...
This Information Applies To: 5200, 5300 and 5400 Fragment Analyzer, Femto Pulse and ZAG DNA analyzer
Issue
When no data is available in the Agilent ProSize data analysis software for one or more capillaries, the capillary(ies) could be misaligned...
This Information Applies To: Agilent ICP-MS (7800/7850/7900/8900)
Issue
How to check the MS40+ or MS40-S foreline pump to determine if the pump needs maintenance?
Background
The oil's cleanliness and level, in the MS40+ or MS40-S foreline...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
Powering on Agilent ICP-MS Systems after maintenance, long-term shutdown, or for power cycling.
Steps to Follow
Confirm that the ICP-MS power plug...