Thank you very much.
We actually monitor mass 56 (among with others) at the beginning of each session because mass 56 counts start at around 30-70 K (skipping warm up, just when the plasma lights up) and go down till ~500 counts in around 20-40 minutes…
For WinUV 5.1.3.1042 SCM has an E-sign option, which says to go to the profile screen which does not have 'Authorize Worksheet' and 'Review Worksheet' Privileges to select….Kind of a wild goosechase.
Click 'Configuration > Electronic Signature' to access…
Here are the services I suspect are not running after your last reboot. Another reason is that the graphing options are available and graphics and annotation are not from the SDA.
Hello,
Thanks for your reply.
I tried the Area Sum option, it works indeed as areas for all transitions are summed, but the chromatograms are still separated for every transition, and thus my S/N is not better. Same thing for the group function, I…
In Agilent GPC/SEC software it is the Coefficient of Determination that can be interpreted as correlation coefficient (r) and this is the parameter that we use to measure the "goodness " of fit.
We have 6546 QTOF in house, however the ion counts of the samples are very low. It is a new instrument and I am expecting E7-E8 signal intensity. Any thoughts here?.
Thanks for the feedback. We were looking at the glass wool with unpacked liner tubes as the cost is greatly different. However when observing how well a prepacked liner compares to one of our techs liners, they look not as secured or dense opposed to…
The mass calibration/check for the quadrupole is failing across all isolation widths. Mass delta on 322m/z exceeds limits.
We system tuned a few weeks ago. Can someone please outline the troubleshooting workflow for this type of issue (where to start…
This Information Applies To: 5975 and 5977 GC/MS systems with MassHunter Acquisition software
Issue:
High-quality GC/MS data requires a low, and stable background of air and water present in the MS analyzer.
This article demonstrates a systematic...
This Information Applies To: Agilent 5975 and 5977 GC/MSD systems with MassHunter Acquisition software
Issue:
High-quality GC/MS data requires a low, and stable background of air and water present in the MS analyzer. This article describes how to...
This Information Applies To: Agilent 5977A/B GC/MSD with MassHunter GC/MS Acquisition Software
Issue:
This article describes the procedure to safely vent (shut down) the 5977A/B GC/MSD with Electron Ionization (EI)
The MSD will be damaged by incorrect...
This Information Applies To: HES ion source in 5977B/C GC/MSD, 7010 triple quadrupole GC/MS systems
Issue
The filaments are replaced as part of routine maintenance, or when they break (zero output current).
Items Required
Gloves, nylon,...
This Information Applies To: Agilent 5977A/B/C GC/MSD
Issue
The Electron Multiplier Horn must be replaced when it is contaminated or the EMV value reaches 3000 V with a clean ion source.
Items Required
Electron multiplier horn (5977B/C:...
This Information Applies To: Agilent 5973/ 5975/5977 GC/MSD with rotary vane foreline pump
Issue:
The oil mist filter is recommended to be replaced annually. If the color of the filter has changed or there is smell from the filter, the oil mist...
This Information Applies To: Agilent EI Source
Issue:
During normal operation of the GC/MS, the EI SST/Inert ion source will need to be disassembled to proceed with abrasive ion source cleaning and / or routine replacement of consumable parts (filaments...
This Information Applies To: Agilent G7129A/B/C Vialsampler
Issue:
Replacing the needle and needle seat of the Vialsampler is required when:
The needle is visibly damaged.
Leaks or blockages in the vialsampler are observed, especially between...
This Information Applies To: Agilent G1311A/B/C, G7111A/B, Quaternary Pumps, and G1310A/B, G7110B Isocratic Pumps, G1312A/B/C, G7112B Binary Pumps
Issue:
How to diagnose no flow or no pressure issues on binary, quaternary, or isocratic pumps.
...
This Information Applies To: Agilent UV and RID detectors
Issue
A clogged flow cell causes high backpressure. The clog can be removed by flushing the system with solvents at high pressure. If you suspect a clog or experience high backpressure due...