My cary 5000 UV-VIS-NIR shows Error code 9:9339SEQ NIR wavelength calibration failed and 9:9303SEQ Unable to initialize the instrument. What is wrong with this machine and how could I fix the problem. Thanks a lot for your advice in advance. MK
Hello, thanks, we are using the version A.04.09 Agilent OpenLAB CDS. And yes, RSDRtDimethyl ist the optional variable Name from the Summary Calculations (RSD from Retention Time). The RSD (from Summary Calc) Format is a Number with 3 Decimal Places. I…
I have been working on an old VWD that was not used much. After running the intensity it failed only on the minimum with a 400 of >6400 cts. So more water was flushed through it over night and the same fail reoccurred. Rebuilt the cell using the g1314…
Hi James, Just a followup on this. I changed the Lan adapter with G1530-62010. However, I still had a deconnexion this weekend and when sending a ping to the GC, the response time is random and high (between 1ms to sometimes 32ms). Is there anything else…
It is really rare that the transferline itself fails. It's a brazement attached to the MS with three bolts and an O ring seal. The transferline column nut threads get messed up if the column nut is overtightened. Using a 10x32 die to clean the threads…
I have recently ran two standards on the Cary 630 FT-IR using the ATR module - qualitative search. One is Heptanes and the other is N-Heptane.
I then ran four samples - three were N-Heptane, the other was Heptanes and compared them to the two standards…
Hi,
I am currently running a USP <467> protocol which monitors the recovery of: methanol, ethanol, acetone, isopropyl alcohol, hexanes, and toluene. I make a standard solution using DMAC with known amounts of solvent and use the same solution to spike…
I went through everything I could find, but it appears that BootP doesn't work properly in Windows 10 and even when you follow the instructions it fails. As I mentioned above, the only way I found to get it working was to replace the JetDirect card with…
You can definitely set up an intelligent report to do what you want, but there is a much easier way to do this in OpenLAB ChemStation. When you create a calibration table, ChemStation gives you an option to 'Calculate Signals Separately': When selected…
I have Chemstation C.01.08 [210]. Whenever I try to run a partial sequence, I get the 'Initialization of Sequence Failed' error message. From what I could find online, that issue was supposed to be solved in C.01.08 version of the software. I have Unique…
This Information Applies To: Agilent 5000 Series ICP-OES Instruments
Issue
The spectrometer incorporates interlocks and covers that are used to monitor critical operations to ensure Operator and instrument protection. If the instrument is used in...
This Information Applies To: Agilent ICP-OES Systems (700 Series, 5000 series)
Issue
If any yellow or orange coloration on any part of the torch is observed (not due to the sample being presented or recently run) or if the torch appears to be visibly...
This Information Applies To: Agilent 700 Series ICP-OES Systems
Issue
The 700 Series ICP-OES requires regular maintenance, and routine maintenance tasks are able to be performed by the instrument operator.
Any maintenance procedures not...
This Information Applies To: Agilent 5000 Series ICP-OES (5100/5110/5800/5900)
Issue
Correct ventilation is required to ensure proper function of the ICP-OES.
Resolution
The ICP-OES must be located under a flue that is vented by an exhaust...
This Information Applies To: Agilent demountable torches
Issue
The Agilent 5000 series ICP-OES instruments can be fitted with a demountable, semi-demountable, or bonded torch. The demountable and semi-demountable torches can be disassembled for...
This Information Applies To: 5100, 5110, 5800, and 5900 ICP-OES instruments
Issue
The ICP-OES operator can identify the source of plasma ignition failure. The main cause is air entering the plasma.
Steps to follow
Excessive air entering...
This Information Applies To: Agilent ICP-OES 5000 Series (5100/5110/5800/5900)
Issue
How to run the ICP-OES Performance Test after installation, preventative maintenance, repairs, and when troubleshooting.
Steps to Follow
The ICP-OES Performance...
This Information Applies To: Agilent 5000 Series ICP-OES
Issue
Blocked nebulizers are the source of many instrument performance issues including loss of sensitivity and poor precision, especially when running organics, high solids, or high salt...
VGA Setup
Multiple Results
This Information Applies To: Agilent VGA 77 (Vapour Generation Accessory)
Issue: This article discusses the setup steps for the VGA 77.
VGA 77
Warning : Noxious Fumes and Corrosive Liquids. Vapor generation methods of analysis involve...
This Information Applies To: Agilent VGA 77 Accessory
Issue: The Agilent Vapor Generation Accessories use high concentrations of HCl and require thorough cleaning to maintain optimum working condition.
Warning : The Vapor Generation...