Thank you for your advice. Unfortunally not only EM test failed but several others as well. we tried to run it last,first, and even not to run it at all
The GC Calculators and Method Translation Software (MTS) is available for download from Agilent.com . The package includes:
The Vapor Volume Calculator . It can be used to determine the expansion volume of a GC sample solvent at a given inlet temperature…
Hi, Here's a screenshot of the system suit, there is no blank subtraction The analyst said he has used the same processing method for a different run with no issues the only difference being that for those runs the MS setting was the same time as the…
The basic tools I would recommend to have for GC maintenance:
Ceramic column cutter
1/4" wrench (column nuts)
7/16" wrench (gas fittings at back of GC)
1/2" wrench (replace gold seal on S/SL inlet)
Torx 20 driver (removing FID collector assembly…
Agilent GC 7890A, FID, Split Liner. I'm setting up the column to do Hexane injection testing. It was set up this way previously but the program had been deleted and the column removed before I started here. Front Detector/Column which is below baseline…
When you say that there are no signs of a leak, have you run a pump leak rate test using Agilent Lab Advisor? If not, I would suggest testing this. If you're unlucky enough for your peak to elute just at the point when the outlet ball valve fails to close…
Hello and Help!
My GC-FID's inlet pressure stays at 0.7 psi and does not reach the setpoint of 10 psi. Makeup gas reaches the 25 psi setting. Liner and septa are fine. I unscrewed the inlet column nut and placed my finger at the bottom of the inlet…
I'm going to be calibrating for ethanol on my HS-GC-FID 6890, but I'm having discrepancies between two standards. The standard that I will be calibrating with (Restek's Residual Solvents #1 34105) is 3000ug/mL in N,N-Dimethylacetamide. I'm verifying the…
Hello,
My laboratory runs a multilevel calibration with internal standards on a headspace-GC-FID. Our sequence is set up to replace each level of the curve after each calibrator is analyzed and then calculate the concentration of the analyte with the…
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
The torch, bonnet, and platinum shield plate must be installed after performing maintenance, or replacing with new components.
Items Required
Standard...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
The torch, bonnet, and shield plate must be removed and inspected during routine maintenance, and when troubleshooting plasma ignition problems. Faults with...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
This procedure tests for an air leak in the sample introduction system, or fault with spray chamber draining, by sealing the end of the torch with a piece...
This Information Applies To: 7700, 7800, 7850, 7900 Agilent ICP-MS instruments
Issue
Error messages related to gas flows can cause the plasma to shut off or disable plasma ignition.
The troubleshooting procedure in this article is applicable for...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
Error messages related to water flow or water valve issues can cause the plasma to shut off or disable plasma ignition. While a warning message will still...
This Information Applies To: Agilent Fluorescence Detectors (FLD)
Issue
Sometimes it’s necessary to change FLD EX and EM wavelengths during a run since not all components will excite or emit at the same wavelengths. However, when the wavelength...
This Information Applies To: Agilent Analytical Scale LC Systems
Issue
To troubleshoot high backpressure within an HPLC system, it’s necessary to understand the expected pressure throughout an operating system. The total pressure for an LC is measured...
This Information Applies To: Agilent LC Samplers except dual needle multisamplers
Issue
High pressure in the LC sampler is sometimes due to a clog in the needle seat assembly, the needle, or the sample loop. The needle can pick up sample particulates...
This Information Applies To: All OpenLab CDS ChemStation Edition software-Standalone Workstation
Issue
After launching OpenLab ChemStation Online, the following error is shown: “ChemStation ChemMain has stopped working” . OpenLab ChemStation Online...
This Information Applies To: Agilent AriaMx, Software version 1.8 and later
Issue
The Aria Warm up Feature was introduced with Aria SW/FW 1.8 to reduce baseline drift. The warm-up feature is used to speed up the heating process that would normally...