How do you split the sample? Is it two different injection ports? Two different columns into the injection port? Or a two way splitter - purged or unpurged?
Are you injecting split or splitless? Please upload the acqmeth.txt file that is in Windows…
Hello,
Error 1213 typically comes with other errors that truly describe the issue, like the 2150 error you are getting.
First, check the cone orifices. Use a microscope or powerful magnifying glass. If they are clogged or salted over, clean. The opening…
This may be due to several factors. First of all, make sure that all plasma monitor connections and cables are properly connected and not damaged. Also check that there is sufficient gas flow (eg argon) to maintain the plasma. Check the cleanliness and…
Hello all,
I´m facing a Silicium contamination in ICP-MS analysis, I have used a 7800 ICP-MS.
I have digested my samples with HF, HCL and HNO3 and neutralized it with boric acid, after the analysis I have Silicium CPS has increased around 30%.
…
Hi Layden,
your source has died (normal ratio Amps/Volts should be starting at 1.9/2.7). Each year you will find a decline in Amps until it has reached 1.6, then it will give a red bar. In your case it's 0, so the filament is probably broken - your…
I have almost the same system as shown in the picture for over a year now. The application was supplied by Da Vinci Laboratory Solutions in the Netherlands. It is a Mettler TGA 2, with a Gerstel MPS autosampler on a Agilent GCMS(MS) with a CIS injector…
Thank you. I contacted the support. I just had to login into agilent subscribenet and download the latest version after entering the authorization key.
Hello,
That looks like a standard IS calibration using area percent. The purity of the standard can be entered as the compound multiplier. I would start by searching the help for calibration, internal standard, and mass percent calculations. You can…
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
The torch, bonnet, and platinum shield plate must be installed after performing maintenance, or replacing with new components.
Items Required
Standard...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
The torch, bonnet, and shield plate must be removed and inspected during routine maintenance, and when troubleshooting plasma ignition problems. Faults with...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
This procedure tests for an air leak in the sample introduction system, or fault with spray chamber draining, by sealing the end of the torch with a piece...
This Information Applies To: 7700, 7800, 7850, 7900 Agilent ICP-MS instruments
Issue
Error messages related to gas flows can cause the plasma to shut off or disable plasma ignition.
The troubleshooting procedure in this article is applicable for...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
Error messages related to water flow or water valve issues can cause the plasma to shut off or disable plasma ignition. While a warning message will still...
This Information Applies To: Agilent Fluorescence Detectors (FLD)
Issue
Sometimes it’s necessary to change FLD EX and EM wavelengths during a run since not all components will excite or emit at the same wavelengths. However, when the wavelength...
This Information Applies To: Agilent Analytical Scale LC Systems
Issue
To troubleshoot high backpressure within an HPLC system, it’s necessary to understand the expected pressure throughout an operating system. The total pressure for an LC is measured...
This Information Applies To: Agilent LC Samplers except dual needle multisamplers
Issue
High pressure in the LC sampler is sometimes due to a clog in the needle seat assembly, the needle, or the sample loop. The needle can pick up sample particulates...
This Information Applies To: All OpenLab CDS ChemStation Edition software-Standalone Workstation
Issue
After launching OpenLab ChemStation Online, the following error is shown: “ChemStation ChemMain has stopped working” . OpenLab ChemStation Online...
This Information Applies To: Agilent AriaMx, Software version 1.8 and later
Issue
The Aria Warm up Feature was introduced with Aria SW/FW 1.8 to reduce baseline drift. The warm-up feature is used to speed up the heating process that would normally...