My cary 5000 UV-VIS-NIR shows Error code 9:9339SEQ NIR wavelength calibration failed and 9:9303SEQ Unable to initialize the instrument. What is wrong with this machine and how could I fix the problem. Thanks a lot for your advice in advance. MK
Hello, thanks, we are using the version A.04.09 Agilent OpenLAB CDS. And yes, RSDRtDimethyl ist the optional variable Name from the Summary Calculations (RSD from Retention Time). The RSD (from Summary Calc) Format is a Number with 3 Decimal Places. I…
I have been working on an old VWD that was not used much. After running the intensity it failed only on the minimum with a 400 of >6400 cts. So more water was flushed through it over night and the same fail reoccurred. Rebuilt the cell using the g1314…
Hi James, Just a followup on this. I changed the Lan adapter with G1530-62010. However, I still had a deconnexion this weekend and when sending a ping to the GC, the response time is random and high (between 1ms to sometimes 32ms). Is there anything else…
It is really rare that the transferline itself fails. It's a brazement attached to the MS with three bolts and an O ring seal. The transferline column nut threads get messed up if the column nut is overtightened. Using a 10x32 die to clean the threads…
Hi,
I am currently running a USP <467> protocol which monitors the recovery of: methanol, ethanol, acetone, isopropyl alcohol, hexanes, and toluene. I make a standard solution using DMAC with known amounts of solvent and use the same solution to spike…
I have recently ran two standards on the Cary 630 FT-IR using the ATR module - qualitative search. One is Heptanes and the other is N-Heptane.
I then ran four samples - three were N-Heptane, the other was Heptanes and compared them to the two standards…
I went through everything I could find, but it appears that BootP doesn't work properly in Windows 10 and even when you follow the instructions it fails. As I mentioned above, the only way I found to get it working was to replace the JetDirect card with…
I have Chemstation C.01.08 [210]. Whenever I try to run a partial sequence, I get the 'Initialization of Sequence Failed' error message. From what I could find online, that issue was supposed to be solved in C.01.08 version of the software. I have Unique…
You can definitely set up an intelligent report to do what you want, but there is a much easier way to do this in OpenLAB ChemStation. When you create a calibration table, ChemStation gives you an option to 'Calculate Signals Separately': When selected…
This Information Applies To: Agilent 5100, 5110, 5800, and 5900 ICP-OES systems
Issue
When troubleshooting communication issues between Agilent 5000 Series ICP-OES and the instrument controlling computer, it is necessary to know the IP address of...
This Information Applies To: Agilent 5000 series ICP-OES systems
Issue
Poor or high relative standard deviation, or a noisy signal is an indication of poor precision during analysis.
Resolution
There are many potential causes for an instrument...
This Information Applies To: Agilent 5000 series ICP-OES systems
Issue
Instrument calibration (wavelength), detector calibration (dark current, or method calibration (worksheet) failure.
Resolution
There are several reasons why a calibration...
This Information Applies To: Agilent 5000 series ICP-OES
Issue
Exhaust temperature and requirements for laboratory site preparation
Background
Certain parameters will impact the actual temperature of the plasma exhaust. Some of these factors...
This Information Applies To: Agilent 700 Series ICP-OES instruments
Issue:
It is important that a torch alignment is performed to ensure that the optics are optimized and are focused on the analytical zone of the plasma. This alignment procedure...
This Information Applies To: Agilent 5800/5900 ICP-OES
Issue:
The instrument requires clean, dry, noncorrosive air for cooling purposes. The air enters the instrument through an air supply vent located beside the chimney on the top of the instrument...
This Information Applies To: Agilent 5100, 5110, 5800, 5900 ICP-OES systems
Issue
The ICP-OES spray chamber filters the sample droplets created by the nebulizer. Larger droplets fall to the chamber drain, while the smaller droplets are introduced...
This Information Applies To: Agilent 5000 ICP-OES Series and Agilent ICP Expert Software
Issue
How to connect Agilent 5000 series ICP-OES systems to Agilent ICP Expert software via LAN
Steps to Follow
How to connect Agilent 5000 series ICP...
This Information Applies To: 5000 series ICP-OES (5100/5110/5800/5900), ICP Expert
Issue
How to Reset the AVS 6/7 after maintenance or when a red LED is visible
Steps to follow
Tips : Instructions for changing the AVS switching...
This Information Applies To: Agilent 5100, 5110, 5800, 5900 ICP-OES
Issue
The axial pre-optic window needs checking from time to time to ensure it is clean.
If the axial pre-optic window is dirty, it must be cleaned or replaced to ensure adequate...