When running a calibration on the GCMS the internal standard increases the entire time for all of our standards. It goes from around 1.9 million for the bottom of the calibration to 3.2 million. Recent things that we have done that should help eliminate…
Hello, we were not able to tune the instrument at all. There was so much noise at low mass that it fails the initial quad coarse mass calibration. We think it is PEG contamination, possibly also PPG, but a number of masses correspond with sodiated PEG…
Morning, You are correct. I am running OpenLab CDS ChemStation. Rev code = C.01.04 [35]. Intelligent Reporting product version A.01.04.122. The system suitability issue is that I'm only getting the TCD satistical results. The FID result are not printing…
Hello Lars, Thanks for your reply. Unfortunately, there is no flow meter meter installed. So you are saying that, in your case without stopping gas flow before GC injection, you are only getting 1-2% deviation in FID response? If possible could you explain…
The tune evaluation criteria are benchmarks that GCMS instruments typically pass.
"Designed for" and "works with" are two different things. The tune evaluation was created before the Extractor Source and High Efficiency Source. These ion sources get…
Hey Ryan, try the following. Normally, the valve command failed is coming as a result of the position not found. Overtightened screws are a typical result if you have done maintenance before (happened to me the first time...). Tighten the screws each…
I have a G4226A autosampler with a recurring error message. Movement of needle into seat failed [EE 4714, 3204]
This error started after the autosampler had been repaired by a field engineer. The main board had to be replaced; the computer was unable…
Hi I have a very basic question, please correct me if I am wrong. I am using GC 7820 with FID detector. Flow , Pressure everything was set by another technician before I started. I know for Back Detector everything is what is set by the Technician in…
This Information Applies To: Agilent OpenLab ChemStation Edition Software (C.01.xx)
Issue
When your Agilent OpenLab ChemStation Edition software fails to launch with errors " Login failed with the following message: Configuration system failed to...
This Information Applies To: Agilent OpenLab ChemStation Edition Software (C.01.xx)
Issue
Agilent OpenLab ChemStation Edition software fails to launch with error containing the words " Autostart Macro failed ”. This article will provide you some...
This Information Applies To: 5200/5300/5400 Fragment Analyzer, Femto Pulse, ZAG DNA Analyzer and Oligo Pro II instruments, and their respective controller software.
Issue Failed to build pressure error comes up shortly after starting a separation...
This Information Applies To: Agilent 6400 Series triple quadrupole LC/MS systems equipped with a gate valve.
Issue
Removing the Ion Transfer Capillary for maintenance on instruments with gate valve. The gate valve allows ion capillary removal and...
This Information Applies To: Agilent OpenLab ChemStation, Agilent OpenLab CDS, Agilent OpenLab EZChrom
Issue
Due to the license error “ An error occurred connecting to the license server: The desired vendor daemon is down. Check the Imgrd log file...
This Information Applies To: HPLC Advisor app
Issue
Legacy HPLC method needs to be translated to a new column or LC system (HPLC to UHPLC or Analytical to Preparative LC).
Requirements
Install the most recent version of the HPLC Advisor...
This Information Applies To: Agilent 7890 A/B, 8860 and 8890 GC Systems with Split/Splitless (SSL), Multimode (MMI) or Programmable Temperature Vaporization (PTV) Inlets
Issue:
The Inlet Leak & Restriction Test is executed after every inlet maintenance...
This Information Applies To: 5000 series ICP-OES (5100,5110,5800,5900), AVS 4/6/7, ICP Expert version 7.X
Issue
The AVS can contribute to instrument performance issues such as sensitivity and precision. During troubleshooting, bypassing (or skipping...
This Information Applies To: Agilent GC Systems
Issue
Loss of peak resolution can be a combination of decrease in separation and increased peak width. Loss of resolution can impact on analytical reproducibility and accuracy.
Other chromatographic...
This Information Applies To: Agilent GC Systems
Issue
Contamination that creates ghost and carry over peaks can be introduced at different points including sample preparation, introduction, and separation. The additional peaks can cause false positive...