5181-1267 - plunger tip material - stainless steel. I'd switch to a PTFE tipped plunger like 5181-3354 . Using water as the last rinse may be the culprit. I've known of this problem happening on Monday after a syringe sits after just water in it from…
What acquisition software are you running? I'm not able to locate that specific error message in the help in MSD Chemstation E.02.02 SP2 nor MassHunter...
A simple troubleshooting step is to remove the syringe and try it.
Hello,
Do you see any errors in the sequence log during the reprocessing? What happens if you process with a new method, can you update the RTs in a new clean method?
Marty
Agilent offers the ADM Flow Meter (G6691A) with replaceable calibrated cartridges. The Flow Meter has a black-and-White digital display and works with acoustic displacement measurement.
The firmware can be updated by connecting the ADM Flow Meter to…
Hello, the small volume webinar at the below link has discussion of one implant using Apparatus 7.
Dissolution: FoundationBeyond (on24.com)
If you'd like to reach out to dissolution.hotline@agilent.com we can discuss further more specifically for…
If the RedCargo site is not available for you or has problems, you can get the ADM Flowmeter Certificate of Calibration Addendum here. The tool uses a print popup, so allow popups for this site.
Certificates of Calibration Addendum
…
Hello,
I want to make transfer from one system to another that has higher dwell volume.
What I know is that the new system should have injection time delay to prevent dwell volume incompatibilities.
I have two questions:
1) In some HPLC C.01…
What could be causing the appearance of that ghost peak?
Analysis on a GTA120 240Z AA
The peak on the left is the peak of interest; the peak on the right is the ghost peak
Analyzing Lead in Blood, I get a graph like the previous one and I have…
This Information Applies To: Agilent Liquid Chromatography (LC) systems
Issue:
Shutting down the HPLC for a long period requires following this general procedure to prevent damage to the system and the column.
Steps to follow:
Store the...
This Information Applies To: Agilent G7129A/B Autosampler with Sample Thermostat/Cooler G7167-60101 or G7167-60005.
Issue:
The autosampler may stop working from time to time, potentially giving off loud noises and switching off the light. The only...
This Information Applies To: Agilent 5977A/B GC/MSD with EI source, EI Extractor Source, or CI Source.
Issue:
During normal operation of the GC/MSD, the source will require cleaning. It is time to clean the source when:
There is a loss in analyte...
This Information Applies To: Agilent HES source, Agilent 5977 Series GC/MSD
Issue:
During normal operation of the GC/MSD, the source will require cleaning. It is time to clean the source when:
There is a loss in analyte response not improving...
This Information Applies To: Agilent 5977 and 5975 Series GC/MSD systems
Issue
The autotune fails and reports the error Tune action stopped: Gain and offset = 0 and peaks are too narrow!
Resolution
The MSD autotune program is run after routine...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
Condition new or cleaned ICP-MS skimmer cones and sampler cones by aspirating a Conditioning Solution before use.
Background
Drift up can be a sign of...
Turn On the GC/MS Interface and Oven Using OpenLab CDS
Multiple Results
This Information Applies To: Agilent GC/MS instruments controlled by OpenLab CDS software
Issue
Turning on the GC/MS interface heater and Oven using OpenLab CDS software.
Steps to Follow
From the Home tab, click Method > Instrument Setup...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900)
Issue
The signal monitor function in MassHunter can help with troubleshooting low sensitivity, carry over, contamination, or high background. It can also be used to optimize...
This Information Applies To: Agilent UV detectors (Variable Wavelength Detectors, Multiple Wavelength Detectors, and Diode Array Detectors)
Issue
Checking accumulated hours on the UV lamp.
Steps to Follow
There are four ways to check the accumulated...
This Information Applies To: Agilent 7700/7800/7850/7900/8800/8900 ICP-MS
Issue:
Poor internal standard (ISTD) mixing can cause high relative standard deviation (RSD).
The recommendations in this article are applicable if:
It takes a long...