If you use diagnostics to fill and dispense to "sample return" do you see anything coming out of the cannulas? See page 61 Agilent 850-DS Dissolution Sampling Station Operator's Manual
Here are some other resources you may find helpful:
Cleaning Validation…
Hi j esus5802
You can try in Previous Results tap /Highlight the spectrum for changing sample name/
Go to view/ then click Data Handling/ enter new sample ID name in the field sample id name/
click on back/ and go to re-Analyze
Select a method…
Hi rahmicetinkaya
We do not have a user manual for a cary 630 FTRI gas cell module,. I have attached some explanations about the use of the gas cell. Hope it helps you
Thanks
Regards
Hi Ardalan.P
Did you change the computer or the computer name?
You can copy license file from "C:\ProgramData\Varian\Cary License.lic" into WinUV folder "C:\Program Files (x86)agilent\Cary WinUV\",
if you change the computer you should find the…
This video guides you through the process of replacing the Electron Multiplier Horn for the Ultivo (G6465A, G6465B), iQ (G6160A).
This video is intended to support the written instructions found in the online help or in your Instruments User Guide.…
This video guides you through the process of replacing the oil and filter for the MS120 pump and applies to G6495 models with an MS120 pump.
This video is intended to support the written instructions found in the online help or in your instrument's…
This video guides you through the oil and filter change process for the MS40+ pump and applies to all LC/MS models equipped with an MS40+ pump.
This video is intended to support the written instructions found in the online help or in your instrument…
This video guides you through the process of removing or installing the nebulizer and applies to all LC/MS models.
This video is intended to support the written instructions found in the online help or in your instrument's user guide.
Parts required…
This Information Applies To: Agilent Liquid Chromatography (LC) systems
Issue:
Shutting down the HPLC for a long period requires following this general procedure to prevent damage to the system and the column.
Steps to follow:
Store the...
This Information Applies To: Agilent G7129A/B Autosampler with Sample Thermostat/Cooler G7167-60101 or G7167-60005.
Issue:
The autosampler may stop working from time to time, potentially giving off loud noises and switching off the light. The only...
This Information Applies To: Agilent 5977A/B GC/MSD with EI source, EI Extractor Source, or CI Source.
Issue:
During normal operation of the GC/MSD, the source will require cleaning. It is time to clean the source when:
There is a loss in analyte...
This Information Applies To: Agilent HES source, Agilent 5977 Series GC/MSD
Issue:
During normal operation of the GC/MSD, the source will require cleaning. It is time to clean the source when:
There is a loss in analyte response not improving...
This Information Applies To: Agilent 5977 and 5975 Series GC/MSD systems
Issue
The autotune fails and reports the error Tune action stopped: Gain and offset = 0 and peaks are too narrow!
Resolution
The MSD autotune program is run after routine...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
Condition new or cleaned ICP-MS skimmer cones and sampler cones by aspirating a Conditioning Solution before use.
Background
Drift up can be a sign of...
Turn On the GC/MS Interface and Oven Using OpenLab CDS
Multiple Results
This Information Applies To: Agilent GC/MS instruments controlled by OpenLab CDS software
Issue
Turning on the GC/MS interface heater and Oven using OpenLab CDS software.
Steps to Follow
From the Home tab, click Method > Instrument Setup...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900)
Issue
The signal monitor function in MassHunter can help with troubleshooting low sensitivity, carry over, contamination, or high background. It can also be used to optimize...
This Information Applies To: Agilent UV detectors (Variable Wavelength Detectors, Multiple Wavelength Detectors, and Diode Array Detectors)
Issue
Checking accumulated hours on the UV lamp.
Steps to Follow
There are four ways to check the accumulated...
This Information Applies To: Agilent 7700/7800/7850/7900/8800/8900 ICP-MS
Issue:
Poor internal standard (ISTD) mixing can cause high relative standard deviation (RSD).
The recommendations in this article are applicable if:
It takes a long...