Using Windows Explorer, underneath your run method's subdirectory is a file called ACQMETH.TXT. Please copy and paste the contents of that file here and we can go over the run parameters.
Do you have a very stable standard to run to ensure your system…
Hello,
That looks like Chemstation in the integrator preview window can you relay the version and confirm the table captured. If that is the case these are preliminary results from the integrator preview for final values, I would look at the reports…
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GC Inlet Maintenance
Find links and part numbers to the consumables used in the video here.
GC Septum
Inlet septa are used to maintain a leak-free seal at the GC inlet, even after repeated injections.
If the septum has a dimple, the dimple…
Modern labs are constantly looking for opportunities to improve their efficiency and reduce the workload of their staff. Automating repetitive tasks can help to maximize instrument usage and free up operators to perform other tasks, improving overall…
Unless you are strictly matrix matching your calibration standards to your samples, it is best to use an internal standard to account for matrix effects. This is standard practice in ICP-OES. Most people use Yttrium or Scandium, an element that is not…
A new educational page from Agilent’s Liquid Chromatography experts is now available. The brand-new HPLC Fundamentals page is curated specifically for scientists wanting to know more about HPLC technology. It also provides answers for HPLC related frequently…
This Information Applies To: Agilent 5975 and 5977 series GC/MSD
Issue:
Tuning the Agilent GC/MSD with EI sources, requires the use of perfluorotributylamine (PFTBA). The calibration vial will be depleted eventually due to regular use. This article...
This Information Applies To: Agilent 5975 and 5977 series GC/MSD
Issue:
If the PFDTD signal is absent or low, but the reagent ions are normal, you may have run out of CI Calibrant.
Inspect the calibration vial on the back of the flow controller...
This Information Applies To: Agilent 5975 and 5977 Series GC/MSD
Issue:
For some GC/MSD maintenance or repair asks, it is required to open the side plate (filament exchange, ion source cleaning, electron multiplier exchange, column installation...
This Information Applies To: Agilent GC/MS MassHunter Acquisition Software Agilent 5975/5977 GC/MSD
Issue
Use the Early Maintenance Feedback (EMF) tool to track the GC/MSD's consumable resource and part use, and to configure alerts for when they...
This Information Applies To: Agilent GC/MSD systems
Issue:
After a filament fails, there will be a system error message: "No emission current". Switching to the other filament (except for the CI ion source, which has just one filament), and then...
This Information Applies To: Agilent 7693A automatic liquid sampler tray
Issue:
The orange Align Mode light comes on . T he sample tray of the Agilent automatic liquid sampler 7693A will not operate again until the alignment procedure has successfully...
This Information Applies To: Agilent 7693A Automatic Liquid Sampler
Issue:
The automatic liquid sampler may need to be replaced, in case it is worn or dirty.
Steps to follow
To remove the syringe:
Open the injector door.
Slide...
This Information Applies To: Agilent 7693A Automatic Liquid Sampler
Issue:
Two turrets are provided with the 7693A injector, the 16-sample standalone turret, and the 3-sample transfer turret used with the 150-sample tray (See Figure 1 ). The turret...
This Information Applies To: Agilent 7697A Headspace Sampler
Issue:
There is a potential leak external to the Headspace unit that can cause loss of pressure.
Steps to Follow:
This article is a troubleshooting guide for when you suspect there...
This Information Applies To: Agilent 7693A Automatic Liquid Sampler
Issue:
This document explains how to replace the syringe carrier assembly in case you want to change from standard to high volume syringes, or if an Agilent support representative...