INSTRUMENT CONTROL PARAMETERS: GCMS-04 -----------------------------------------
C:\MSDCHEM\1\METHODS\60m_VOLITILES_230511_1.M Tue May 30 13:44:52 2023
Control Information ------- -----------
Sample Inlet : GC Injection Source : GC ALS Mass Spectrometer…
It's best to set the system to vent and turn off the power first. You do not need to actually vent it/open the MS.
Lift off the analyzer cover as shown.
Remove the three T-20 screws at the red arrows.
Then the entire side panel will pivot out…
Related question. Simple GC with a valco rotary valve, 10 position, 6 position, whatever. what is the scfm requirement for that pneumatic device over the course of a method run where after half a minute the valve switches, then 15 minutes later switches…
Good afternoon everyone,
We are performing the media replacement accuracy test in our 850-DS Dissolution Sampler Station and our test is failing (specification <=9mL), as per table below:
Friday Run:
#
Initial Weight
Final Weight
Difference…
Hi everyone, hoping I can get some help with this, as I've tried many solutions and so far nothing has worked longer than a few hours. I'm running at 7890A with 5975C MS. Yesterday morning, Instrument Control froze after running our opening standards…
I have been using Chemstation with my Agilent 7890/5975C for a few years now. I closed down the software and machine to perform a source cleaning.
Now, when I attempt to open Chemstation it state: "GC error: CreateNotificationHost() in InitializeDevice…
By chance is your TCD plumbed to your FID, non destructive to destructive detector configuration? Or using a splitter device of some type? A picture from inside the oven would help. Have you tried the split vent maintenance yet? I would do this even without…
It is only possible to subtract a background spectrum from a TIC in MSD ChemStation (File > Subtract Background (BSB) ), not an entire blank run's chromatogram. If this is data being collected by a 2D GC detector (FID, ECD, etc...) then you can use the…
Error : Data Subscriptions Failed. Are inbound Ports Blocked? Is there Right Type of GC at IP Address? GC does seem to be connected but not the MS. Does anyone have suggestions on what the problem might be?
This Information Applies To: Agilent GC Systems with Flame Ionization Detector (FID)
Issue:
The Flame Ionization Detector (FID) jet could become clogged with ferrule material, column bleed, or heavy molecular analytes. The clogged jet will affect...
This Information Applies To: Agilent GC Systems with Split/Splitless (S/SL) inlet
Issue
Different liners are required for different high concentration, split analysis techniques including:
General use liners
Auto inject, general use
Auto...
This Information Applies To: Agilent GC Systems with Split/Splitless (S/SL) inlet
Issue
Different liners are required for different splitless trace analysis techniques including:
General use liners
Pressure, temperature, volume (PTV)
Hot...
This Information Applies To: Agilent 6890, 7890, 7820, 8890 and 8860 GC Systems with Split/Splitless (S/SL) inlet
Issue
Replacement of the Gold Seal is required as part of inlet maintenance. Replacement is required when the performance of the inlet...
This Information Applies To: Agilent GC Systems with Micro-ECD.
Issue
The Wipe Test is an annual test that performed by end user of the micro-ECD (Micro Electron Capture Detector or uECD) to help ensure radioactive safety when using the detector...
This Information Applies To: Agilent GC Systems with thermal conductivity detector (TCD)
Issue
Baking the thermal conductivity detector (TCD) at high temperatures can remove sample contaminants that have deposited on the detector surfaces.
Items...
This Information Applies To: Agilent GC Systems with flame ionization detector (FID)
Issue
Baking out the flame ionization detector at high temperatures can remove sample contaminants that have deposited on the detector surfaces.
Items required...
This Information Applies To: Micro Electron Capture Detector (uECD)
Issue
Baking the micro electron capture detector (µECD) at high temperatures can remove sample contaminants that have deposited on the detector surfaces.
Warning ...
This Information Applies To: Agilent GC Systems with Flame Ionization Detector (FID)
Issue
This article will describe how an operator can configure the makeup gas on both the instrument keypad and the software driver (Method Editor).
Background...
This Information Applies To: Agilent HPLC systems
Issue
The presence of ghost peaks can be a symptom of a system contamination issue, caused by accumulation of sample and/or foreign substances in the flow path. It is critical for high sensitivity...