Hi.
So ive had a very high sample with Methanol (around 8000 mg/l) and now i still have contamination around 500 mg/l in my blanks. Ive tried injecting IPA and replaced the syringe. Any other tips? Ive also pumped up the oven/column tempature to a…
5 psi inlet pressure running hydrogen with your configuration leads to 2.3 ml/min to the MS and 1.02 ml/min to the FID.
You are welcome. Are you using a two-hole ferrule in the injection port or a splitter of some type? The two-holed ferrules are..…
Hello,
3-way valve is a good idea, but unfortunately all I had was several 5180-4160 Tee, 1/8 in, brass, and several 0100-2144 Ball valve, 1/8 inch.
So I decided to make following setup.
In the setup below I am using He as carrier gas and N2 as…
Hello Agilent Users,
Im missing a feature in Openlab since day 1. How do I override and start a run if the GC is not ready ?
For example: the FID temperature is set at 250°C in the method and the actual temperature is at 220°C (it is still heating…
Is there a table / document somewhere on what Agilent GC FID flows I should be using for a particular column ? Right now I have a 7890B with a 30m 0.32 column film thickness 0.25. We use it for petroleum / Diesel Range Organic analysis with a ALS injector…
Hi,
My baseline is around 8pA in standby state. H2 is coming from a tank and I can rule out contaminations in the gas source because the gas line is splitted with T piece: one is going to the FID EPC and one is going to the inlet PCM. H2 is the carrier…
Canadian_Chemist ,
There is an example of printing text instead of the final concentration based on the LOQ outlier in this discussion.
(+) Report builder - Final Concentration Expression Change - Forum - Mass Spectrometry Software - Agilent Community…
The GC counter rolls over at 999,999...but 100,542 is still a lot!
Great drawing, thanks. That setup makes it difficult to figure out pressures/flows. The path of least resistance is all of the 530 pieces unless the methanizer and the connection from…
The idea behind the multiple modes is to keep the flows going through your FID constant. Changing flows will change the flame characteristics and cause the baseline to shift. Some suggestions:
If your column is set to constant flow mode, use "Constant…
This Information Applies To: Agilent 4200, 4150 and 2200 TapeStation.
Issue
Is it possible to analyze single stranded DNA (ssDNA) on the TapeStation? Which kit is the most suitable for analysis of ssDNA?
Resolution
Agilent does not offer any...
This Information Applies To: Agilent 4200 and 4150 TapeStation systems
Issue
How to Run the software installation verification on 4200 and 4150 TapeStation systems.
Background
The 4150 TapeStation model G2992A and 4200 TapeStation model G2991B...
This Information Applies To: Agilent 5200/5300/5400 Fragment Analyzer, and Femto Pulse
Issue
Perform a capillary alignment when a new array is installed in your Agilent Parallel Capillary Electrophoresis instrument. An alignment may also be performed...
This Information Applies To: Agilent 4200 and 4150 TapeStation
Issue
Are the Agilent DNA and RNA ScreenTape assays denaturing?
Resolution
The DNA ScreenTape assays in the TapeStation portfolio are not denaturing. Only the RNA and High Sensitivity...
This Information Applies To: Agilent LC pumps with manual purge valve.
Issue
A good practice before using a system is to purge the system to remove air. This is done by observing the clear tubing from the solvent bottle as well as the waste line...
This Information Applies To: ICP-MS MassHunter 4.x and 5.x
Issue
Unable to open a batch in offline data analysis, or the batch is empty.
If the ICP-MS MassHunter software closes unexpectedly, there is a power outage, or the ICP-MS and computer...
This Information Applies To: Agilent OpenLab CDS versions 2.4 or higher.
Issue
How to preview result files using various Report Templates in OpenLab CDS versions 2.4 or higher.
Requirements
The user has the result set loaded in OpenLab CDS...
This Information Applies To: ICP-MS MassHunter with Spectroscopy Database Administrator (SDA) and Protect Local Data ON.
Issue
An 'Authentication failed' error message appeared after entering user name and password when attempting to download a...
This Information Applies To: ICP-MS MassHunter with Spectroscopy Database Administrator (SDA) and Protect Local Data On.
Issue
With Spectroscopy Database Administrator (SDA) and Protect Local Data turned on, batches are not accessible through file...
This Information Applies To: Agilent AriaMx real-time PCR system
Issue
Scratches on AriaMx optical modules can lead to a reduction in their performance.
Background
Scratches on an AriaMx optical module are shown in Figure 1 .
Figure 1 ....