INSTRUMENT CONTROL PARAMETERS: GCMS-04 -----------------------------------------
C:\MSDCHEM\1\METHODS\60m_VOLITILES_230511_1.M Tue May 30 13:44:52 2023
Control Information ------- -----------
Sample Inlet : GC Injection Source : GC ALS Mass Spectrometer…
It's best to set the system to vent and turn off the power first. You do not need to actually vent it/open the MS.
Lift off the analyzer cover as shown.
Remove the three T-20 screws at the red arrows.
Then the entire side panel will pivot out…
Related question. Simple GC with a valco rotary valve, 10 position, 6 position, whatever. what is the scfm requirement for that pneumatic device over the course of a method run where after half a minute the valve switches, then 15 minutes later switches…
Hi everyone, hoping I can get some help with this, as I've tried many solutions and so far nothing has worked longer than a few hours. I'm running at 7890A with 5975C MS. Yesterday morning, Instrument Control froze after running our opening standards…
Good afternoon everyone,
We are performing the media replacement accuracy test in our 850-DS Dissolution Sampler Station and our test is failing (specification <=9mL), as per table below:
Friday Run:
#
Initial Weight
Final Weight
Difference…
I have been using Chemstation with my Agilent 7890/5975C for a few years now. I closed down the software and machine to perform a source cleaning.
Now, when I attempt to open Chemstation it state: "GC error: CreateNotificationHost() in InitializeDevice…
By chance is your TCD plumbed to your FID, non destructive to destructive detector configuration? Or using a splitter device of some type? A picture from inside the oven would help. Have you tried the split vent maintenance yet? I would do this even without…
It is only possible to subtract a background spectrum from a TIC in MSD ChemStation (File > Subtract Background (BSB) ), not an entire blank run's chromatogram. If this is data being collected by a 2D GC detector (FID, ECD, etc...) then you can use the…
Than you should probably stop advertise it as a sulfur-specific filter on specs table (add "and hydrocarbons" words) https://www.agilent.com/en/products/lab-supplies/chromatography-spectroscopy/gas-management/gas-clean-purification-syste… . Otherwise…
This Information Applies To: Agilent 7890 A/B, 8860 and 8890 GC Systems with Split/Splitless (SSL), Multimode (MMI) or Programmable Temperature Vaporization (PTV) Inlets
Issue:
The Inlet Leak & Restriction Test is executed after every inlet maintenance...
This Information Applies To: 5000 series ICP-OES (5100,5110,5800,5900), AVS 4/6/7, ICP Expert version 7.X
Issue
The AVS can contribute to instrument performance issues such as sensitivity and precision. During troubleshooting, bypassing (or skipping...
This Information Applies To: Agilent GC Systems
Issue
Loss of peak resolution can be a combination of decrease in separation and increased peak width. Loss of resolution can impact on analytical reproducibility and accuracy.
Other chromatographic...
This Information Applies To: Agilent GC Systems
Issue
Contamination that creates ghost and carry over peaks can be introduced at different points including sample preparation, introduction, and separation. The additional peaks can cause false positive...
This Information Applies To: Agilent GC Systems
Issue
Several problems can be identified in GC chromatograms, and each of these problems can have various different sources.
Regular maintenance of your instrument in accordance with the recommended...
This Information Applies To: Agilent OpenLab CDS software
Issue
This article describes how to troubleshoot initialization errors during start of OpenLab CDS Data Analysis software. These troubleshooting steps will recreate the OpenLab CDS user.config...
This Information Applies To: Agilent SIPS 10/20 and Flame AA
Issue
Replacing and conditioning the SIPS pump tubing.
Background
Whenever new pump tubes have been installed, it is necessary to condition the tubing before the analysis to prevent...
This Information Applies To: OpenLab CDS software versions 2.1 to 2.5
Contents
This article describes how to process a calibration with disabled calibration points in OpenLab CDS software versions 2.1 to 2.5.
Background
In OpenLab CDS software...
This Information Applies To: OpenLab CDS version 2.6 or later.
Contents
This article describes how to process a calibration when some calibration points have been disabled, using OpenLab CDS software version 2.6 or later.
Background
In previous...
This Information Applies To: Agilent OpenLab CDS
Issue
Outlining the step-by-step instruction on how to integrate peaks using Integration Events in Processing Method.
Background
Integration locates the peaks in a signal and calculates their...