That is one failure mode of Platinum Resistance Thermometers. It can happen one degree to the next higher degree. The heater/sensor must be replaced, part number G1099-60107.
See also: (+) AUX 2 heater fault - Forum - GC/MS - Agilent Community
Hello,
My concern with chromatographic blank subtraction has to do more with the chromatography shifting in RT. When that happens even if the blank peak is smaller than the peak in the standard or sample it can shift enough to cause artifacts on your…
Yup, this seems like it'd be a super useful feature, except you'd have to make sure your CPS are adjusted for every batch after you calibrate. It would be nice to be able to just use the calibration curve for your batch
Hi, I don't think it is a fault of the purity of the solvent. This is normal when using acetonitrile. If you are using an iso pump to dose your reference masses, increase the flow rate, as the gradient rises. Another option is to change the mobile phase…
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Method and Application Review of ASTM D5185 for the Analysis of Used and Unused Lubricating and Base Oils by Inductively Coupled Plasma Atomic Emission Spectrometry on…
I am not aware of any default 'oxide' conversion in MassHunter.
Titanium requires HF to remain stable in solution. A linear high-bias across the entire calibration range could indicate that titanium was lost (low) in your calibration standards. Easy…
This Information Applies To: Agilent OpenLab CDS 2.x
Issue
This article outlines the step-by-step instruction on how to overlay chromatograms for OpenLab CDS 2.x
Steps to Follow
Load data from result sets or single samples. See Load or add...
This Information Applies To: Agilent Lab Advisor Software, Agilent Multicolumn Thermostat
Issue:
Agilent Lab Advisor is a great tool to diagnose the issue of your HPLC. Running the tests that are relevant to your specific issue in the Service &...
This Information Applies To: Agilent OpenLab CDS (ver 2.x)
Content:
The following procedure shows how to review completed injections in a running sequence in OpenLab CDS (ver 2.x).
Steps to Follow:
Select the sequence from the Run Queue...
This Information Applies To: Agilent Liquid Chromatography (LC) systems
Issue:
Shutting down the HPLC for a long period requires following this general procedure to prevent damage to the system and the column.
Steps to follow:
Store the...
This Information Applies To: Agilent G7129A/B Autosampler with Sample Thermostat/Cooler G7167-60101 or G7167-60005.
Issue:
The autosampler may stop working from time to time, potentially giving off loud noises and switching off the light. The only...
This Information Applies To: Agilent 5977A/B GC/MSD with EI source, EI Extractor Source, or CI Source.
Issue:
During normal operation of the GC/MSD, the source will require cleaning. It is time to clean the source when:
There is a loss in analyte...
This Information Applies To: Agilent HES source, Agilent 5977 Series GC/MSD
Issue:
During normal operation of the GC/MSD, the source will require cleaning. It is time to clean the source when:
There is a loss in analyte response not improving...
This Information Applies To: Agilent 5977 and 5975 Series GC/MSD systems
Issue
The autotune fails and reports the error Tune action stopped: Gain and offset = 0 and peaks are too narrow!
Resolution
The MSD autotune program is run after routine...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
Condition new or cleaned ICP-MS skimmer cones and sampler cones by aspirating a Conditioning Solution before use.
Background
Drift up can be a sign of...