The probability of water precipitation is very low if the FID temperatures are high enough, but in times of 5890 the FID could not ignite well when water was present. In principle a FID can be operated without makeup gas, which manufacturers officially…
I was experiencing ghost peaks in my water blank shots so I decided to do some maintenance. This included a new S/SL liner and septum, removing the first inch or two of the column, FID disassembly and ultrasonic cleaning of the jet, and reassembly. Now…
Hello Samehalsharawy ,
Can you please elaborate on the statement we uninstalled the cylinder expecting the flow to come down to zero but it didn't. It stayed at 50?
If no physical tank is connected to the GC, the GC gas connections are capped…
I have a problem with my FID on a HP-4890d Gas Cromatograph.
The FID was working as normal, then the FID didn't start, so I checked the gas flows, and the H2 didn't come out from FID.
I suspect maybe the Hydrogen pipe line is clogged or the on/off…
Hi Marty,
We have a FID and an MS connected to the same system. We only want to acquire the signal of FID, but if we want to report the method parameters we are “forced” to acquire both (we do not really know why and we have already ask the question…
Part Number
Description
Link to Ordering (includes photo)
126 1012
J&W DB-1 GC Column, 10 m, 0.05 mm, 0.05 µm, 7 inch cag
126-1012 | Agilent
5182 0717
Cap, screw, blue, PTFE/red silicone septa, 100/pk. Cap size: 12 mm
5182-0717…
Hi all,
We have a 5975 MSD that is failing to pump down. The turbo pump (Pfeiffer HiPace 300) does not appear to be spinning up, though the turbo pump electronic drive unit has power and is displaying LED light activity. The rough pump has been serviced…
Learn about how to inspect the torch, bonnet, shield plate, and RF Coil, as well as torch cleaning and handling recommendations for Agilent ICP-MS systems.
Preventative and regular maintenance are crucial in avoiding ignition issues and plasma instability…
Hi, thank you for your reply.
I am trying to process metabolomic sample .d files generated from an LCMS-QTOF. I did not get this problem a month ago, however, to solve other problems with permissions I had to uninstall and reinstall profinder.
I have…
Why noise? I don't see a problem with noise.
With regards to the failed drift results, officially the test is to be run with a flow rate of 0.5 ml/min.
This Information Applies To: Agilent 5975 and 5977 series GC/MSD
Issue:
Tuning the Agilent GC/MSD with EI sources, requires the use of perfluorotributylamine (PFTBA). The calibration vial will be depleted eventually due to regular use. This article...
This Information Applies To: Agilent 5975 and 5977 series GC/MSD
Issue:
If the PFDTD signal is absent or low, but the reagent ions are normal, you may have run out of CI Calibrant.
Inspect the calibration vial on the back of the flow controller...
This Information Applies To: Agilent 5975 and 5977 Series GC/MSD
Issue:
For some GC/MSD maintenance or repair asks, it is required to open the side plate (filament exchange, ion source cleaning, electron multiplier exchange, column installation...
This Information Applies To: Agilent GC/MS MassHunter Acquisition Software Agilent 5975/5977 GC/MSD
Issue
Use the Early Maintenance Feedback (EMF) tool to track the GC/MSD's consumable resource and part use, and to configure alerts for when they...
This Information Applies To: Agilent GC/MSD systems
Issue:
After a filament fails, there will be a system error message: "No emission current". Switching to the other filament (except for the CI ion source, which has just one filament), and then...
This Information Applies To: Agilent 7693A automatic liquid sampler tray
Issue:
The orange Align Mode light comes on . T he sample tray of the Agilent automatic liquid sampler 7693A will not operate again until the alignment procedure has successfully...
This Information Applies To: Agilent 7693A Automatic Liquid Sampler
Issue:
The automatic liquid sampler may need to be replaced, in case it is worn or dirty.
Steps to follow
To remove the syringe:
Open the injector door.
Slide...
This Information Applies To: Agilent 7693A Automatic Liquid Sampler
Issue:
Two turrets are provided with the 7693A injector, the 16-sample standalone turret, and the 3-sample transfer turret used with the 150-sample tray (See Figure 1 ). The turret...
This Information Applies To: Agilent 7697A Headspace Sampler
Issue:
There is a potential leak external to the Headspace unit that can cause loss of pressure.
Steps to Follow:
This article is a troubleshooting guide for when you suspect there...
This Information Applies To: Agilent 7693A Automatic Liquid Sampler
Issue:
This document explains how to replace the syringe carrier assembly in case you want to change from standard to high volume syringes, or if an Agilent support representative...