Thank you very much for your quick attention. I take advice to use Labadvisor, however, the host computer is a windows 7 system and the built-in net framework is NE3.5, but LabAdvisor downloaded from Agilent site needs Net Framework version 4.7.2 , which…
Hello Guys, I am using Agilent 7890a GC with an FID detector. I using this GC in online mode to analyze reactor exit gases. I am currently studying the dehydrogenation of Methylcyclohexane over Pt catalyst. Recently I noticed that the FID response is…
Hi All,
We have a 5977 MSD which came up with two errors following a site power outage:
"Source Heater Error: Timeout - temperature fails to increase under full power." "Analyser Heater Error: Timeout - temperature fails to increase under full power…
I am new to GC. I am trying to make a calibration table for a set of fatty acid standards using Agilent 8860 (GC-FID)
After the derivitization step, analysis of the resulting methyl esters shows only the solvent peak. Usually a very high solvent peak…
First off, it is not the barcode reading that causes the vial leaking, but my best guess is that the barcode reading introduces a variable time, that then can cause a scheduling conflict. This scheduling conflict is then not handled, and the 7697A is…
Hello,
Does anyone know were the signal data for the live signal displayed in the online signal window is stored and/or how to access it in Chemstation Rev.B.04.03[16]? I would like to write a macro to run in the scheduler to periodically grab a live…
We suddenly lost power during sample injection, when the power back, the autosampler got needle lock fail error message and fail to go back to needle seat, anybody could help? we did a cold start but not work.
This is absolutely the wrong column. Ammonia and H2S need apolar thick films to be separated and no specialized Free-Fatty-Acid-Phase (FFAP). A CP-Volamines column would do (CP7448) . Ammonia elutes just after CO2 and before water, H2S after water at…
For the GC-6890 FID detector issues you're experiencing, here's a simplified approach to troubleshoot the errors:
Gas Supplies:
Make sure all gas supplies (utility, makeup, hydrogen) are on.
Check that the pressure…
We have a GC-MA7890B with an FID detector and I are observing spikes in the baseline after we made a couple of changes.
We installed guard columns with unions on inlet and detector side, added a 2nd gas cylinder and required tubing, cleaned the FID…
This Information Applies To: Agilent OpenLab CDS
Issue
Identifying the baseline codes and baseline code descriptions for OpenLab CDS
Background
OpenLab CDS Data Analysis includes the same integration algorithms as available in both OpenLAB...
This Information Applies To: Agilent OpenLab CDS
Issue
This article provides step-by-step instructions to filter a signal in an Intelligent Report.
Requirements
To be able to carry out the procedure as described, the privilege of Data Processing...
This Information Applies To: Agilent OpenLab CDS
Issue
This article outlines different ways to quantify the amount of compound in an unknown sample.
Background
Quantitation uses peak area or height to determine the amount of a compound in...
This Information Applies To: Agilent G1329A/B and G1313A Standard Autosampler
Issue
Replacing the needle seat of the Agilent 1100/1200/1260 Standard Autosampler may be required during regular maintenance, replacing a bent needle, or flow path blockage...
This Information Applies To: Agilent G1329A/B and G1313A Standard Autosampler
Issue
Replacing the needle of the Agilent 1100/1200/1260 Standard Autosampler may be required during regular maintenance, replacing a bent needle, or flow path blockage...
This Information Applies To: Agilent 1290 Infinity (G4226A) and Agilent 1260 Infinity (G1367E) HiP Autosamplers
Issue
Replacing the Needle Assembly of the Autosampler is required when:
The needle is visibly damaged.
Leaks or blockages in the...
This Information Applies To: Agilent 6000 Series LC/MS Systems equipped with MS40+ rotary vane pumps
Issue
Replacing the MS-40+ (rough pump) fluid periodically is a key maintenance procedure to improve vacuum performance and minimize the possibilities...
This Information Applies To: All Agilent 6000 Series LC/MS Systems without a gate valve for ion capillary installation/removal. For instructions for removing an ion capillary on LC/MS instruments with a gate valve installed, please click here
Issue...
This Information Applies To: Agilent 6000 series LC/MS instruments
Issue:
Cleaning the ion transfer capillary as part of regular maintenance or as part of troubleshooting when a loss of sensitivity in the instrument occurs.
Steps to follow ...
This Information Applies To: Agilent 6000 Series LC/MS systems.
Issue
Efficient electrospray ionization (ESI) in your LC/MS ion source requires a properly adjusted nebulizer needle in good condition. The nebulizer needle is a consumable item in...