Hi.
So ive had a very high sample with Methanol (around 8000 mg/l) and now i still have contamination around 500 mg/l in my blanks. Ive tried injecting IPA and replaced the syringe. Any other tips? Ive also pumped up the oven/column tempature to a…
5 psi inlet pressure running hydrogen with your configuration leads to 2.3 ml/min to the MS and 1.02 ml/min to the FID.
You are welcome. Are you using a two-hole ferrule in the injection port or a splitter of some type? The two-holed ferrules are..…
Canadian_Chemist ,
There is an example of printing text instead of the final concentration based on the LOQ outlier in this discussion.
(+) Report builder - Final Concentration Expression Change - Forum - Mass Spectrometry Software - Agilent Community…
Yes, it is off on all gasses, always by roughly 20% (occasionally nearly 30% or as low as 15%, depending on the instrument). Air, Hydrogen, Makeup (N2), carrier (H2 or He) on every instrument (12 GC and 3 GC/MS, which haven't been evaluated). It's also…
Hello,
3-way valve is a good idea, but unfortunately all I had was several 5180-4160 Tee, 1/8 in, brass, and several 0100-2144 Ball valve, 1/8 inch.
So I decided to make following setup.
In the setup below I am using He as carrier gas and N2 as…
When trying to close a connection on an instrument with an active single run or sequence the OpenLAB CDS software will usually give a message that it will close connection when the runs are finished. Today when trying to close 2 instruments on the same…
Hello Agilent Users,
Im missing a feature in Openlab since day 1. How do I override and start a run if the GC is not ready ?
For example: the FID temperature is set at 250°C in the method and the actual temperature is at 220°C (it is still heating…
Hi,
My baseline is around 8pA in standby state. H2 is coming from a tank and I can rule out contaminations in the gas source because the gas line is splitted with T piece: one is going to the FID EPC and one is going to the inlet PCM. H2 is the carrier…
Hi all
Apparently the engineer who did the mainboard replacement made a mistake by plugging the MCGV cable to the SSV cable, this made the valve failed to switch (EE 2040.2) and electronic fuse of SSV (EE2049.0) error always appear. It was out of my…
This Information Applies To: Agilent OpenLab CDS
Issue
Identifying the baseline codes and baseline code descriptions for OpenLab CDS
Background
OpenLab CDS Data Analysis includes the same integration algorithms as available in both OpenLAB...
This Information Applies To: Agilent OpenLab CDS
Issue
This article provides step-by-step instructions to filter a signal in an Intelligent Report.
Requirements
To be able to carry out the procedure as described, the privilege of Data Processing...
This Information Applies To: Agilent OpenLab CDS
Issue
This article outlines different ways to quantify the amount of compound in an unknown sample.
Background
Quantitation uses peak area or height to determine the amount of a compound in...
This Information Applies To: Agilent G1329A/B and G1313A Standard Autosampler
Issue
Replacing the needle seat of the Agilent 1100/1200/1260 Standard Autosampler may be required during regular maintenance, replacing a bent needle, or flow path blockage...
This Information Applies To: Agilent G1329A/B and G1313A Standard Autosampler
Issue
Replacing the needle of the Agilent 1100/1200/1260 Standard Autosampler may be required during regular maintenance, replacing a bent needle, or flow path blockage...
This Information Applies To: Agilent 1290 Infinity (G4226A) and Agilent 1260 Infinity (G1367E) HiP Autosamplers
Issue
Replacing the Needle Assembly of the Autosampler is required when:
The needle is visibly damaged.
Leaks or blockages in the...
This Information Applies To: Agilent 6000 Series LC/MS Systems equipped with MS40+ rotary vane pumps
Issue
Replacing the MS-40+ (rough pump) fluid periodically is a key maintenance procedure to improve vacuum performance and minimize the possibilities...
This Information Applies To: All Agilent 6000 Series LC/MS Systems without a gate valve for ion capillary installation/removal. For instructions for removing an ion capillary on LC/MS instruments with a gate valve installed, please click here
Issue...
This Information Applies To: Agilent 6000 series LC/MS instruments
Issue:
Cleaning the ion transfer capillary as part of regular maintenance or as part of troubleshooting when a loss of sensitivity in the instrument occurs.
Steps to follow ...
This Information Applies To: Agilent 6000 Series LC/MS systems.
Issue
Efficient electrospray ionization (ESI) in your LC/MS ion source requires a properly adjusted nebulizer needle in good condition. The nebulizer needle is a consumable item in...