Hi!
I run 200.8 on the 7850 ICPMS for drinking water.
I calibrate with 10, 50, 100, 250, and 500 ppb for Cu (among others). I would like to calibrate up to 2,000 or higher for Cu - but every time I try to calibrate above 500, my CCV and LFB fail…
Hello I have an ICP-MS 7900. My Check Performace fails all the time. I washed the entire system and replaced the chambers and cone again. The same applies to oil changes. Nevertheless, my Check Performace fails. Can anyone help me with this? Or someone…
Hello
We have an agilent ultivo qqq and last week when trying to run a checktune it failed giving a message saying calibrant bottle is empty or nebulizer is clogged. Nevertheless the calibrant bottle is definitely not empty, and the nebulizer also doesnt…
Hello, I have a G1321B that showed errors during the OQPV. The FSE changed the flash lamp Iand the Intensity test is OK arround 10000 counts buen the and Raman ASTM Signal/Noise fail. I want to know if there are another test to do.
I changed my acquisition method from using front FID to back FID. I changed this in the acquisition method detector, signals, and columns sections. On my status tab, the detector is still showing front FID and the online signals is showing no options…
Hello,
Our lab currently uses a headspace-GC-FID to analyze for ethanol in blood samples. We have a multi-level, internal standard calibration curve as well as control samples at various concentrations that are analyzed in a sequence. Is there a way…
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New Year resolution for my ICP-MS: I will keep my ICP-MS analysis free from contaminants…
Hello lperry ,
The document below explains what that error is, essentially it could be that an ALS is not ready for injection, or some other piece of hardware connected to the GC.
6890 GC Not Ready Messages (agilent.com) (bottom of page 9).
…
Hello,
I am expeirencing the same issue after having to reload E.02.02.1431. The quant report prints as one job and the chromatogram and the spectra reports (I'm printing a detailed report) print as a second job.
I've done as ron_tackett mentioned…
When doing autotune I get high precursor in mass 502. I get 12.79% and the limit is 12%. The manual says that it could be contaminated. The equipment has had preventive maintenance recently but it has now this problem. Previously it had a ratio of mass…
This Information Applies To: Agilent OpenLab CDS (version 2.x)
Contents:
In the following procedure, you will find steps to create a multipoint ESTD calibration method with OpenLab CDS 2.X.
Steps to follow:
1. Load the Data
a. From Data...
This Information Applies To: Agilent MassHunter Quantitative Analysis Software
Issue
Chromatographic peak integration is a critical part of accurate and reproducible quantitative data analysis. The integrator type and the integration parameters...
This Information Applies To: Agilent 6200/6400/6500 Series LC/MS Systems
Issue
Instructions on how to fill the calibrant bottle on 6200/6400/6500 Series LC/MS Instruments when calibrant levels are running low.
Background
The ability to autotune...
This Information Applies To: All Agilent 6000 Series LC/MS Systems without a gate valve for ion capillary installation/removal.
Issue:
Installing the Ion Transfer Capillary after cleaning or replacement. For instructions for installing an ion capillary...
This Information Applies To: AriaMx Real-time PCR System
Issue
The saturation level is unique for each optical module after the offset of calibration factor and background calibration. The FAM, ROX, HEX, CY3 & CY5 optical modules will saturate at...
This Information Applies To: Agilent LC Systems
Issue
While it is possible to combine modules from different HPLC series such as 1100, 1200, 1260 or 1290 series to create a functioning LC system, there are some important topics to consider.
...
Fixes for the "RPC Server Unavailable" Error
Multiple Results
This Information Applies To: Agilent OpenLab CDS
Issue
When launching the instrument Acquisition screen/instrument session, there is an "RPC Server Unavailable" error.
Resolution
Accessing the Services App (Windows)
There are two ways to...
This Information Applies To: Agilent LC Pumps
Issue
If a user suspects that the gradient composition isn’t accurate and causes poor chromatography such as retention time shifts, late, early, no peaks or merging peaks. This article provides a quick...
This Information Applies To: Agilent 1290 Infinity (G4226A) and Agilent 1260 Infinity (G1367E) HiP Autosampler
Issue
Replacing the Needle Seat of the Autosampler is required when:
The needle seat is visibly damaged.
Leaks or blockages in the...
This Information Applies To: Agilent OpenLab CDS
Issue
This article discusses different types of bracketing modes and how to set up a bracketed calibration in Data Analysis for OpenLab CDS 2.x
Background
Occasionally, the instrument conditions...