5181-1267 - plunger tip material - stainless steel. I'd switch to a PTFE tipped plunger like 5181-3354 . Using water as the last rinse may be the culprit. I've known of this problem happening on Monday after a syringe sits after just water in it from…
What acquisition software are you running? I'm not able to locate that specific error message in the help in MSD Chemstation E.02.02 SP2 nor MassHunter...
A simple troubleshooting step is to remove the syringe and try it.
Hello,
Do you see any errors in the sequence log during the reprocessing? What happens if you process with a new method, can you update the RTs in a new clean method?
Marty
Agilent offers the ADM Flow Meter (G6691A) with replaceable calibrated cartridges. The Flow Meter has a black-and-White digital display and works with acoustic displacement measurement.
The firmware can be updated by connecting the ADM Flow Meter to…
Hello, the small volume webinar at the below link has discussion of one implant using Apparatus 7.
Dissolution: FoundationBeyond (on24.com)
If you'd like to reach out to dissolution.hotline@agilent.com we can discuss further more specifically for…
If the RedCargo site is not available for you or has problems, you can get the ADM Flowmeter Certificate of Calibration Addendum here. The tool uses a print popup, so allow popups for this site.
Certificates of Calibration Addendum
…
Hello,
I want to make transfer from one system to another that has higher dwell volume.
What I know is that the new system should have injection time delay to prevent dwell volume incompatibilities.
I have two questions:
1) In some HPLC C.01…
What could be causing the appearance of that ghost peak?
Analysis on a GTA120 240Z AA
The peak on the left is the peak of interest; the peak on the right is the ghost peak
Analyzing Lead in Blood, I get a graph like the previous one and I have…
This Information Applies To: Agilent GC Systems
Issue
Peak fronting is present in a chromatography peak when it has an excessive asymmetry with a leading edge. A normal peak is almost symmetrical.
Other chromatographic problems are identified...
This Information Applies To: Agilent GC Systems
Issue
A shift in retention time can occur for single, multiple or all peaks.
Other chromatographic problems are identified in Basic Troubleshooting for GC Systems . Regular maintenance of your instrument...
This Information Applies To: Agilent GC Systems
Issue
A change in peak size can occur for single, multiple or all peaks.
Other chromatographic problems are identified in Basic Troubleshooting for GC Systems . Regular maintenance of your instrument...
This Information Applies To: Agilent GC Systems
Issue
Peak splitting is when a single compound is shown in the chromatogram as two peaks usually unresolved, or one of the peaks is a shoulder.
Other chromatographic problems are identified in Basic...
This Information Applies To: Agilent GC Systems
Issue
This test isolates the point of contamination to the sample introduction system, which includes the gas supply, gas supply lines, and the sample inlet. It does not include the syringe or autosampler...
This Information Applies To: Agilent GC systems
Issue
Peak tailing is present in a chromatography peak when it has an excessive asymmetry with a trailing edge. A normal peak is almost symmetrical.
Other chromatographic problems are identified...
T his Information Applies To: Agilent 8890/8860/7890/7820/6850/6890 GC Systems with TCD (Thermal Conductivity Detector)
Issue
Problems observed with thermal conductivity detector (TCD) results can have different underlying causes.
Resolution...
This Information Applies To: All GCs, 6890, 6850, 7890, 7820, 8890/8860, Intuvo 9000
Issue:
This article is a troubleshooting guide for when the Flame Ionization Detector (FID) does not ignite or the flame keeps going out.
Cause:
If the FID...
This Information Applies To: Agilent GC Systems with Flame Ionization Detector (FID)
Issue:
The Flame Ionization Detector (FID) jet could become clogged with ferrule material, column bleed, or heavy molecular analytes. The clogged jet will affect...
This Information Applies To: Agilent GC Systems with Split/Splitless (S/SL) inlet
Issue
Different liners are required for different high concentration, split analysis techniques including:
General use liners
Auto inject, general use
Auto...