Hi azrael, The FID is not a pressurized detector so there is no pressure test. You may wish to explore our GC Fundamentals series on our website. See Below for a link Fundamentals of Gas Chromatography (GC) - Part 1 | Agilent Regards James
Hi fabiotestoni , From the log file it appears the issue is with one of Qual's dependencies, SQL Server Compact Edition [09AC:06F0][2020-03-11T21:11:48]i301: Applying execute package: SSCERuntime_x64, action: Install, path: C:\ProgramData\Package Cache…
We have a 7890B that was configured with an MSD but is being reconfigured for a different analysis. It is now running an FID/TCD method, and the aux detector has been disconnected and unconfigured. The MS/Aux Det button on the GC keyboard says no aux…
Hi This morning the check Tune failed. After adjusting MS1, the tune passed with warnings. Then I decided to autotune. It went through many of the steps until "Enhanced" failed. I am not sure what this step is. Not easy to find any documentation. Can…
Hello,
I am having an issue getting the system pressure test to pass. I have referred to the manual and followed all the steps, and have checked for any leaks (there are no visible leaks) and the leak test on the system is also passing - yet the pressure…
When Air gap is 0.2 and the flow rate is 2.1 ml/min then the peak area found 287 by FID but when the air gap is 0 and flow rate is 1.47 ml/min then the area reduced to 141. Where analysis performed by Autosampler.
Hello everyone
I have 3 error messages from the Agilent infinity ii 1260 SFC Multi sampler:
1- Metering device Movement Failed ( EE25444.0) 2- Taking needle From park station failed ( EE25105.201 ) 3- Axis did not reach its target position in time…
I think we do this at my lab but not with a valve. We use a plot column and anayze headspace above a water sample. We test for methane ethane ethene and propane useing an FID. The integrated gastight syringe with a valve in it from Fisher helps. We use…
Using OpenLab EZChrom A.04.1.0.0 with a 6890N GC-FID this error occurs
The IS dept have looked into this and have commented that the systems log mentions that the instance has reached its maximum size of 32MB. We have been running the same system…
Hi, I have the same problem as well. We are using LC 1220 Infinity series. We tried flushing the system with isopropanol for 10 minutes just in case the bubbles are present. However, this does not solve the problem. The pump failed to get ready within…
This Information Applies To: Agilent Atomic Absorption Spectroscopy Systems (240/280 Series Flame AA and 240/280Z/Zeeman/GTA 120 Graphite Furnace)
Issue:
This article includes recommended maintenance procedures to be performed daily, weekly or annually...
This Information Applies To: Agilent SpectrAA Software, Agilent 240/280 Flame Atomic Absorption Systems, 240/280 Zeeman Graphite Furnace Systems
Issue:
How to Reset Lamp Usage Counters or Add a New Lamp in SpectrAA
Caution : All physical...
This Information Applies To: Agilent GTA 120, Agilent 240Z AA Spectrometer, Agilent 280Z AA Spectrometer, Agilent 240FS/GTA120/PSD120/UltrAA System
Issue:
It is important to align the sample probe of the Programmable Sampler Dispenser (PSD) 120...
This Information Applies To: Agilent Flame AA Systems: e.g., 55B, 240FS, 280FS
Issue:
The Flame AA burner and burner components require regular cleaning to maintain system performance. Components include the burner, nebulizer, and spray chamber...
This Information Applies To: Agilent Flame Atomic Absorption (AA) Spectrometers (50/55/240/280 AA)
Issue:
How to clean a blocked nebulizer of a Flame AA, which may be causing low sensitivity or a sample uptake rate below 5 ml/min.
Steps to follow...
This Information Applies To: Agilent Graphite Furnace Systems (PSD 120/GTA 120/240Z AA/280Z AA)
Issue
Maintenance procedure for replacing the syringe and plunger of the PSD 120 sample dispenser for the Agilent GTA and Zeeman Graphite Furnace Systems...
This Information Applies To: Agilent AA (AA240, AA280) with Graphite Furnace Accessory (GTA)
Issue:
The Programmable Sample Dispenser (PSD) requires the sampling probe to be accurately aligned before the PSD can be used.
The PSD enables the...
This Information Applies To: All Agilent AA systems: 55B, 240FS, 280FS, 240Z, 280Z
Issue:
Optimizing the position of the lamp maximizes amount of light from the lamp passing through the optics to the detector, improving the signal-to-noise and the...
This Information Applies To: Agilent VGA 77, AA, VGA 77P, ICP
Issue:
The Agilent Vapor Generation Accessories VGA 77 and VGA 77P use high concentrations acids. The system needs to be thoroughly cleaned after each use.
The Vapor Generation Accessory...
This Information Applies To: All Agilent Atomic Absorption Spectrometry Systems (AA50, AA55, AA240, AA280)
Issue: This article describes when and how to clean an AA burner.
Background
For optimum and safe performance, burners (see Figure 1 ...