Hi joonseok
Put the samples in a separate sequence to the wash runs. In the sequence parameters for the samples, select the post sequence option to switch off the lamps. Run the sample sequence and queue up the wash sequence from the Run control menu…
Hello,
I have a question about our GC 8860, which has been experiencing some problems since I changed the valve pressure.
Although it works well immediately after the change, if I don't use the GC for a few days, the first few runs produce larger…
Hi Everyone,
Due to random readings of my samples, i ran wavelength and photometric accuracy test. Both of them fails, do i need to replace the lamp or is it because of the wavelength drive gear?
thanks.
When the tuning is done at 3200 (+) everything is fine. When I change it to tune at 1700 (+) the masses are reasonably accurate. After it gets to the third mass (620) it appears that the entire spectrum shifts by about 1.5 AMU and the tuning fails. There…
If you want to know what specific module is sending a Leak error, this article in the Knowledge Portal can help:
Determining which Module is Causing the Shutdown Error Due to a Leak
The "Valve command failed transport command failed" Error can have…
The optional high vacuum gauge has a cable between the gauge and the electronics. It is either disconnected or the gauge has failed.
See page 125 and 126 in the 5977B Series MSD Operating Manual for instructions on how to turn it on and off.
The…
There is an SP7 switching valve on our 5110 ICP-OES The first set of triplicate aspirations of Std always ride really close to the precision limit of 2%RSD and then std#2 and Std3 are typical 0.5 or less. (ISTD Method) All of these standards are in the…
I have a 7820A GC connected to a 5977B MS. When I submit a sample, it injects and runs as normal at first. Near the end of the run, an error message pops up that reads "Attempt to download method to GC failed." Additionally, when I check the logbook,…
Hi everybody, firstly, excuse me for my english. Please I need a video about how to install AJS and MMI in qtofms 6545, because we have a tune problem when we use MMI, (tune failed). To autotune the system, we need to remove MMI and install AJS. Any suggestions…
Hi All, I need help to fix either baseline drifted down or change volume injection of water samples in GC/FID. Specifically, I am setting up a new GC instrument for analysis of methanol and alcohols in water samples with the following conditions: - Instrument…
This Information Applies To: Agilent Atomic Absorption Spectroscopy Systems (240/280 Series Flame AA and 240/280Z/Zeeman/GTA 120 Graphite Furnace)
Issue:
This article includes recommended maintenance procedures to be performed daily, weekly or annually...
This Information Applies To: Agilent SpectrAA Software, Agilent 240/280 Flame Atomic Absorption Systems, 240/280 Zeeman Graphite Furnace Systems
Issue:
How to Reset Lamp Usage Counters or Add a New Lamp in SpectrAA
Caution : All physical...
This Information Applies To: Agilent GTA 120, Agilent 240Z AA Spectrometer, Agilent 280Z AA Spectrometer, Agilent 240FS/GTA120/PSD120/UltrAA System
Issue:
It is important to align the sample probe of the Programmable Sampler Dispenser (PSD) 120...
This Information Applies To: Agilent Flame AA Systems: e.g., 55B, 240FS, 280FS
Issue:
The Flame AA burner and burner components require regular cleaning to maintain system performance. Components include the burner, nebulizer, and spray chamber...
This Information Applies To: Agilent Flame Atomic Absorption (AA) Spectrometers (50/55/240/280 AA)
Issue:
How to clean a blocked nebulizer of a Flame AA, which may be causing low sensitivity or a sample uptake rate below 5 ml/min.
Steps to follow...
This Information Applies To: Agilent Graphite Furnace Systems (PSD 120/GTA 120/240Z AA/280Z AA)
Issue
Maintenance procedure for replacing the syringe and plunger of the PSD 120 sample dispenser for the Agilent GTA and Zeeman Graphite Furnace Systems...
This Information Applies To: Agilent AA (AA240, AA280) with Graphite Furnace Accessory (GTA)
Issue:
The Programmable Sample Dispenser (PSD) requires the sampling probe to be accurately aligned before the PSD can be used.
The PSD enables the...
This Information Applies To: All Agilent AA systems: 55B, 240FS, 280FS, 240Z, 280Z
Issue:
Optimizing the position of the lamp maximizes amount of light from the lamp passing through the optics to the detector, improving the signal-to-noise and the...
This Information Applies To: Agilent VGA 77, AA, VGA 77P, ICP
Issue:
The Agilent Vapor Generation Accessories VGA 77 and VGA 77P use high concentrations acids. The system needs to be thoroughly cleaned after each use.
The Vapor Generation Accessory...
This Information Applies To: All Agilent Atomic Absorption Spectrometry Systems (AA50, AA55, AA240, AA280)
Issue: This article describes when and how to clean an AA burner.
Background
For optimum and safe performance, burners (see Figure 1 ...