Hi danielchsny , Yes power spikes from unscheduled power interruptions can cause damage to sensitive electronic circuits. Another contributing factor is that when power is lost to the LC/MS running under high vacuum the rough pump will stop, causing a…
Hi Carol_Ultivo , There is always a trade-off or balance to be struck between Scan speed, mass resolution and sensitivity in any quadrupole mass filter. So, if you decrease the resolution and keep scan speeds the same you will naturally get an increase…
Yes - it was a bit of a mess - but I was able to fix it. Thanks for the heads up. Not everything could be fixed in the computer portion of the method. I had to go into the GC configuration and fix it there.
Thank you!
Thank you for the suggestions. Yes, some of what I'm doing does not require the ISTD but I leave it in the analysis method b/c of needing it in some of the work. I haven't had a chance to work on this in a couple of weeks, but will definitely keep it…
Hello Adrsto ,
I apologize for the delayed repsonse.
It is not possible to use the NIST algorithm itself within Unknowns Analysis. As you mentioned, you can adjust the forward and reverse settings and enable the Adjust Score option, which from the…
Hello Lstephan ,
I apologize for the delayed response.
Errors of this type generally point to an issue with a preferences file. The first thing to try is clearing these using the Restore User Settings tool found in the Quant Tools group in the start…
Hello AJohnson13 ,
This is a known issue if Acquisition has been pinned to the Windows Taskbar and run from there in MassHunter Acq Version 11.x and later. This is due to the OpenLab integration and the need to launch through Control Panel to include…
Please give more information. TSU - is that Thermal Screening Unit? You say under varying pressures...from zero to how many PSI/Bar? Will you need to use a vacuum to get the sample? Will this be analytes in air or something else? Decomposition of what…
This Information Applies To: Agilent Atomic Absorption Spectroscopy Systems (240/280 Series Flame AA and 240/280Z/Zeeman/GTA 120 Graphite Furnace)
Issue:
This article includes recommended maintenance procedures to be performed daily, weekly or annually...
This Information Applies To: Agilent SpectrAA Software, Agilent 240/280 Flame Atomic Absorption Systems, 240/280 Zeeman Graphite Furnace Systems
Issue:
How to Reset Lamp Usage Counters or Add a New Lamp in SpectrAA
Caution : All physical...
This Information Applies To: Agilent GTA 120, Agilent 240Z AA Spectrometer, Agilent 280Z AA Spectrometer, Agilent 240FS/GTA120/PSD120/UltrAA System
Issue:
It is important to align the sample probe of the Programmable Sampler Dispenser (PSD) 120...
This Information Applies To: Agilent Flame AA Systems: e.g., 55B, 240FS, 280FS
Issue:
The Flame AA burner and burner components require regular cleaning to maintain system performance. Components include the burner, nebulizer, and spray chamber...
This Information Applies To: Agilent Flame Atomic Absorption (AA) Spectrometers (50/55/240/280 AA)
Issue:
How to clean a blocked nebulizer of a Flame AA, which may be causing low sensitivity or a sample uptake rate below 5 ml/min.
Steps to follow...
This Information Applies To: Agilent Graphite Furnace Systems (PSD 120/GTA 120/240Z AA/280Z AA)
Issue
Maintenance procedure for replacing the syringe and plunger of the PSD 120 sample dispenser for the Agilent GTA and Zeeman Graphite Furnace Systems...
This Information Applies To: Agilent AA (AA240, AA280) with Graphite Furnace Accessory (GTA)
Issue:
The Programmable Sample Dispenser (PSD) requires the sampling probe to be accurately aligned before the PSD can be used.
The PSD enables the...
This Information Applies To: All Agilent AA systems: 55B, 240FS, 280FS, 240Z, 280Z
Issue:
Optimizing the position of the lamp maximizes amount of light from the lamp passing through the optics to the detector, improving the signal-to-noise and the...
This Information Applies To: Agilent VGA 77, AA, VGA 77P, ICP
Issue:
The Agilent Vapor Generation Accessories VGA 77 and VGA 77P use high concentrations acids. The system needs to be thoroughly cleaned after each use.
The Vapor Generation Accessory...
This Information Applies To: All Agilent Atomic Absorption Spectrometry Systems (AA50, AA55, AA240, AA280)
Issue: This article describes when and how to clean an AA burner.
Background
For optimum and safe performance, burners (see Figure 1 ...