HPLC 2024 will be held from July 20-25 , 2024 in Denver , Colorado this year. We will host our Reach Your Summit Reception which will be held on July 23 rd from 6pm – 8pm local time at Earl’s Kitchen + Bar. At this event, you will find different areas…
Hello Ruthvn Please share some photos of your chromatograms and check for void volumes in capillary connections. Once the issue occurs, does it keep occurring for subsequent injections or do the resolution and acceptable peak shape come back in later…
Hello LCMSvsLCUV Would you be able to share more details about what you are trying to achieve please, including the instrument set up, application, analyte of interest and the column part number?
We are having a issue clearing up these valleys/dips after our peaks of interest. So far we have confirmed no leaks up to the column (pressure and leak test passed), new column, new guard column, new mobile phases, new standards, and several purges through…
Hello,
I will assume you mean you are using the backup restore tool for CDS 2.4 not the ECM XT import scheduler. If you have setup an import scheduler task to back the ECM-XT system up that would be self-referential and would not actually back anything…
Hello,
Although limited Chemstation does save some confg files and other information at the OS user level, so creating a new OS user would clear those files. Also, some printer configurations can cause problems with Chemstation as it tries to read…
The Agilent range of UV-Vis/NIR spectrophotometers cater to a variety of analytical needs, from routine applications to high-end experiments. UV-Vis/NIR instruments can perform a range of measurements in rechargeable battery research, including quantitative…
This Information Applies To: Agilent Liquid Chromatography (LC) systems
Issue:
Shutting down the HPLC for a long period requires following this general procedure to prevent damage to the system and the column.
Steps to follow:
Store the...
This Information Applies To: Agilent G7129A/B Autosampler with Sample Thermostat/Cooler G7167-60101 or G7167-60005.
Issue:
The autosampler may stop working from time to time, potentially giving off loud noises and switching off the light. The only...
This Information Applies To: Agilent 5977A/B GC/MSD with EI source, EI Extractor Source, or CI Source.
Issue:
During normal operation of the GC/MSD, the source will require cleaning. It is time to clean the source when:
There is a loss in analyte...
This Information Applies To: Agilent HES source, Agilent 5977 Series GC/MSD
Issue:
During normal operation of the GC/MSD, the source will require cleaning. It is time to clean the source when:
There is a loss in analyte response not improving...
This Information Applies To: Agilent 5977 and 5975 Series GC/MSD systems
Issue
The autotune fails and reports the error Tune action stopped: Gain and offset = 0 and peaks are too narrow!
Resolution
The MSD autotune program is run after routine...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
Condition new or cleaned ICP-MS skimmer cones and sampler cones by aspirating a Conditioning Solution before use.
Background
Drift up can be a sign of...
Turn On the GC/MS Interface and Oven Using OpenLab CDS
Multiple Results
This Information Applies To: Agilent GC/MS instruments controlled by OpenLab CDS software
Issue
Turning on the GC/MS interface heater and Oven using OpenLab CDS software.
Steps to Follow
From the Home tab, click Method > Instrument Setup...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900)
Issue
The signal monitor function in MassHunter can help with troubleshooting low sensitivity, carry over, contamination, or high background. It can also be used to optimize...
This Information Applies To: Agilent UV detectors (Variable Wavelength Detectors, Multiple Wavelength Detectors, and Diode Array Detectors)
Issue
Checking accumulated hours on the UV lamp.
Steps to Follow
There are four ways to check the accumulated...
This Information Applies To: Agilent 7700/7800/7850/7900/8800/8900 ICP-MS
Issue:
Poor internal standard (ISTD) mixing can cause high relative standard deviation (RSD).
The recommendations in this article are applicable if:
It takes a long...