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Hi Micela,
Try to double-check the standard creation. I see at the point of std 1 it is not good. And make sure in the measurement delay 45>60-70s, to ensure the sample / std reacts perfectly.
If using an autosampler change the measurement 45>90s. Because I see a large rsd where usually the reaction has not stabilized. I recommend Sncl2.
Hi Micela,
Try to double-check the standard creation. I see at the point of std 1 it is not good. And make sure in the measurement delay 45>60-70s, to ensure the sample / std reacts perfectly.
If using an autosampler change the measurement 45>90s. Because I see a large rsd where usually the reaction has not stabilized. I recommend Sncl2.