the abundance of ion 69. I rechecked the source and it doesn't look dirty. then I did an autotune it stopped on the width mass axis of the second quadrupole.
Finally, after 2 or 3 more attempts, I ended up completing the autotune with an abundance of…
Hi all,
I am currently troubleshooting a leaky 1260 infinity II HPLC-SFC-ELSD and want to carry out a leak test in the utility program, but i could not find a clear, detailed description on how to do this. Could anyone direct me to the correct resource…
Hi!
I still need help yes, please!
- On the machines (GC system and Injector) it just says HP6890 (see photos attached)
- The PC we employ is an old Windows XP running one, that was used to run the GC-FID before we want to control it with the serial…
Hi, I would suggest to test the same without column installed to the FID. If problem looks similar check for leaks at the FID gas lines and clean the FID. If not clean the inlet and replace the split vent line and filter. Maybe try a new column.
BR…
Hi there, I noticed recently that the ECD back signal on Agilent GC 7890 (using it for trace gas analysis) is oddly spiking (while the FID is a straight, consistent line). It never used to do this. I just recently changed the inlet septum, could this…
Hi Community
I have an Issue on one of our GC-FIDs 6890N. I have large Peak Tailing, especially on the back of my chromatogramm:
What i already did:
- New Column
- New Septa/liner
- New Gold Plate
- Cleaned Inlet and Detector
- Re…
I have a Cary 3500 and running Cary UV Workstation Software 1.2 and Windows 10
I downloaded the new Cary UV Workstation Software 1.3 via the Agilent SubscribeNet.
first I ran the systemPreparationTool.exe
That finished without issues.
Then I ran…
*The system and method are given at the bottom of this post*
I am working with an Agilent 8860 operating a DB-624 UI (30m x 0.25mm x 1.4um) column with nitrogen carrier gas and split inlet (20:1). The system was shut down for approximately 1 year, and…
Any special procedures to prepare for cross-country shipment a 7890B with SS, PP inlets, heated valve oven, and TCD-FID? Also a 7697A with 100-vial tray?
Turning off the systems on Friday night that need to be ready to go on Monday morning is not recommended. It can take quite some time for a GC/MS to come back up to operational after being shut down. Even cooling the temperatures all down and then heating…
This Information Applies To: Agilent OpenLab CDS (version 2.x)
Contents:
In the following procedure, you will find steps to create a multipoint ESTD calibration method with OpenLab CDS 2.X.
Steps to follow:
1. Load the Data
a. From Data...
This Information Applies To: Agilent MassHunter Quantitative Analysis Software
Issue
Chromatographic peak integration is a critical part of accurate and reproducible quantitative data analysis. The integrator type and the integration parameters...
This Information Applies To: Agilent 6200/6400/6500 Series LC/MS Systems
Issue
Instructions on how to fill the calibrant bottle on 6200/6400/6500 Series LC/MS Instruments when calibrant levels are running low.
Background
The ability to autotune...
This Information Applies To: All Agilent 6000 Series LC/MS Systems without a gate valve for ion capillary installation/removal.
Issue:
Installing the Ion Transfer Capillary after cleaning or replacement. For instructions for installing an ion capillary...
This Information Applies To: AriaMx Real-time PCR System
Issue
The saturation level is unique for each optical module after the offset of calibration factor and background calibration. The FAM, ROX, HEX, CY3 & CY5 optical modules will saturate at...
This Information Applies To: Agilent LC Systems
Issue
While it is possible to combine modules from different HPLC series such as 1100, 1200, 1260 or 1290 series to create a functioning LC system, there are some important topics to consider.
...
Fixes for the "RPC Server Unavailable" Error
Multiple Results
This Information Applies To: Agilent OpenLab CDS
Issue
When launching the instrument Acquisition screen/instrument session, there is an "RPC Server Unavailable" error.
Resolution
Accessing the Services App (Windows)
There are two ways to...
This Information Applies To: Agilent LC Pumps
Issue
If a user suspects that the gradient composition isn’t accurate and causes poor chromatography such as retention time shifts, late, early, no peaks or merging peaks. This article provides a quick...
This Information Applies To: Agilent 1290 Infinity (G4226A) and Agilent 1260 Infinity (G1367E) HiP Autosampler
Issue
Replacing the Needle Seat of the Autosampler is required when:
The needle seat is visibly damaged.
Leaks or blockages in the...
This Information Applies To: Agilent OpenLab CDS
Issue
This article discusses different types of bracketing modes and how to set up a bracketed calibration in Data Analysis for OpenLab CDS 2.x
Background
Occasionally, the instrument conditions...