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Back to Basics - IN PERSON - Various Dates
Key Considerations for Dissolution Software and Compliance on May 23
Use of LC-MS/MS Technique for Quantitative Analysis of…
Hi Fury,
Are you using Cary WinUV with the CFR Package which uses CRM? There should be someone who has qualified your system and would also have access. You can also, reinstall the software since there isn't that much to the initial setup if you haven…
Locking does not appear to be designed to lock specific methods as it is to lock the app to prevent say Scan or Kinetics to be used by a second account while the first person is using it.
Hi, Using one and the same column for different applications is possible, as long both solvents are permitted (column user manual e.g.).
The column should always be flushed very slowly from solvent A to B (0.1 mL/min). At least 5 times the column volume…
Hi Marty,
Thanks for taking the time to respond. I saved the data to a file and then printed the file and it was properly formatted. I think that there is an issue with printing to paper from the method. Since this is a long unsupported CS revision…
Hi Abbey
Thanks for the info!
So far we have only been running this on various forms of olive oil. But the waves in the baseline remain regardless of MOAH contant. I have run samples that were analyzed by outside labs (with COA) that contain 0ppm…
This Information Applies To: Agilent GC Systems
Issue
Excessive baseline noise can be introduced at different points including sample preparation, sample introduction, separation, and the detector. The excessive background can cause reduced signal...
This Information Applies To: Agilent GC Systems
Issue
Baseline instability that is not reproducible across multiple runs can be introduced at different points including sample introduction, separation, and the detector. The baseline instability...
This Information Applies To: Agilent GC Systems
Issue
Peak fronting is present in a chromatography peak when it has an excessive asymmetry with a leading edge. A normal peak is almost symmetrical.
Other chromatographic problems are identified...
This Information Applies To: Agilent GC Systems
Issue
A shift in retention time can occur for single, multiple or all peaks.
Other chromatographic problems are identified in Basic Troubleshooting for GC Systems . Regular maintenance of your instrument...
This Information Applies To: Agilent GC Systems
Issue
A change in peak size can occur for single, multiple or all peaks.
Other chromatographic problems are identified in Basic Troubleshooting for GC Systems . Regular maintenance of your instrument...
This Information Applies To: Agilent GC Systems
Issue
Peak splitting is when a single compound is shown in the chromatogram as two peaks usually unresolved, or one of the peaks is a shoulder.
Other chromatographic problems are identified in Basic...
This Information Applies To: Agilent GC Systems
Issue
This test isolates the point of contamination to the sample introduction system, which includes the gas supply, gas supply lines, and the sample inlet. It does not include the syringe or autosampler...
This Information Applies To: Agilent GC systems
Issue
Peak tailing is present in a chromatography peak when it has an excessive asymmetry with a trailing edge. A normal peak is almost symmetrical.
Other chromatographic problems are identified...
T his Information Applies To: Agilent 8890/8860/7890/7820/6850/6890 GC Systems with TCD (Thermal Conductivity Detector)
Issue
Problems observed with thermal conductivity detector (TCD) results can have different underlying causes.
Resolution...
This Information Applies To: All GCs, 6890, 6850, 7890, 7820, 8890/8860, Intuvo 9000
Issue:
This article is a troubleshooting guide for when the Flame Ionization Detector (FID) does not ignite or the flame keeps going out.
Cause:
If the FID...