The tune evaluation criteria are benchmarks that GCMS instruments typically pass.
"Designed for" and "works with" are two different things. The tune evaluation was created before the Extractor Source and High Efficiency Source. These ion sources get…
Hello, we were not able to tune the instrument at all. There was so much noise at low mass that it fails the initial quad coarse mass calibration. We think it is PEG contamination, possibly also PPG, but a number of masses correspond with sodiated PEG…
I have a G4226A autosampler with a recurring error message. Movement of needle into seat failed [EE 4714, 3204]
This error started after the autosampler had been repaired by a field engineer. The main board had to be replaced; the computer was unable…
Hey Ryan, try the following. Normally, the valve command failed is coming as a result of the position not found. Overtightened screws are a typical result if you have done maintenance before (happened to me the first time...). Tighten the screws each…
I am trying to quantify ethyl lactate in ethanol 20% (remainder water). When I run multiple injections, the RSD is 6-8% for the ethyl lactate peak. The ethyl lactate standard should be 0.2% v/v. We typically test samples that are 95-100% ethanol and use…
Hi, I am using Agilent 7820A GC-FID with EZChrom Elite v3.3.2. software. After the completion of each sequence, I would like to automatically generate a .text file along .dat file. So far, after the sequence has ended, I process the sequence and then…
Good Evening, I realize this is a bizzare question but basically what we have is a Dean Switch GCMS system and we use cut windows to determine when the best time is to switch from column 1 (inlet to switch to 3rd column - vent) to column 2 (inlet column…
Hello,
We have an agilent 6545. Today when we are doing a mass calibration check, the masses of the negative tune ions seems to be shifted (For example 1633.9988 is now showing 1639.2109 and so on for the other ions) and mass calibration check seems…
I think that, with this version of the software, there are configuration files stored in the "instrument number folder", e.g. C:\Chem32\n I was going to suggest that you try to delete/rename the config.reg file, having closed all instances of Chemstation…
Actually, you have to be sure that it's detector problem or not.
And if still problem persist and after changing lamps intensity test, wavelength test failed again then you have to call to your local agilent support to check electronics and optics etc…
This Information Applies To: Agilent OpenLab ChemStation
Issue
This article describes the fundamentals of noise determination and calculation in Agilent OpenLab ChemStation to report the signal-to-noise ratio.
Tips : To report the...
This Information Applies To: Agilent OpenLab CDS
Issue
The default workflow for OpenLab CDS is the following: Reprocess Results > Save Results > Print Results . This is the recommended workflow for regulated environments.
For nonregulated environments...
This Information Applies To: ICP-MS MassHunter 4.x/5.x
Issue
Reviewing the latest Performance Report, and Performance Report History is a useful tool for troubleshooting ICP-MS instrument performance issues. Historical sensitivity, background, precision...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
How to perform routine maintenance on the Agilent ICP-MS Torch.
Background
Deposits on the torch can be removed by routine maintenance. Maintenance frequency...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
The torch, bonnet, and platinum shield plate must be installed after performing maintenance, or replacing with new components.
Items Required
Standard...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
The torch, bonnet, and shield plate must be removed and inspected during routine maintenance, and when troubleshooting plasma ignition problems. Faults with...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
This procedure tests for an air leak in the sample introduction system, or fault with spray chamber draining, by sealing the end of the torch with a piece...
This Information Applies To: 7700, 7800, 7850, 7900 Agilent ICP-MS instruments
Issue
Error messages related to gas flows can cause the plasma to shut off or disable plasma ignition.
The troubleshooting procedure in this article is applicable for...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
Error messages related to water flow or water valve issues can cause the plasma to shut off or disable plasma ignition. While a warning message will still...
This Information Applies To: Agilent Fluorescence Detectors (FLD)
Issue
Sometimes it’s necessary to change FLD EX and EM wavelengths during a run since not all components will excite or emit at the same wavelengths. However, when the wavelength...