The Agilent Cary 3500 Flexible UV-Vis system is a versatile instrument used for analyzing a privacy screen's light transmission properties at various angles and light conditions. It boasts a spacious sample compartment suitable for different accessories…
One of the most challenging tasks for vacuum system designers is to create ultra-high and extreme-high vacuum pressures. Pumps capable of generating UHV and XHV pressure include Sputter Ion Pumps, Titanium Sublimation Pumps and Non-Evaporative Getters…
A system with poorly designed conductance can have drastic consequences on the effective pumping speed: the cornerstone of this tutorial is to emphasize the need to design a system that does not have negative effects on the performance of a high or ultrahigh…
Thermal gauges, out of all the available gauge technologies, offer excellent value for measuring rough vacuum pressure, but even UHV and XHV systems can benefit from them. All thermal gauges operate by heating a filament and exposing it to the vacuum…
When detecting leaks, it is important to distinguish between virtual and real ones. Examples of virtual leaks can be: gas desorption, diffusion, trapped volume, and back streaming. Leak-up or rate-of-rise tests can indicate whether a vacuum system's base…
Ionization gauges convert residual molecules to positively charged ions, and then attract them to a negatively charged collector where they create a measurable current. Modifications to high vacuum ionization gauges can optimize their performance at a…
No one gauge technology will provide pressure measurement throughout the range of vacuum. Combining vacuum sensors can produce a gauge capable of measuring pressure better than with any single technology. After having highlighted the properties of individual…
When choosing a vacuum gauge, it is possible to adopt high vacuum ionization gauges or sputter ion current. After describing the basic operating principle of the Sputter ion pump, this video shows how to measure UHV pressure with Agilent SIPs.
This Information Applies To: Agilent Liquid Chromatography (LC) systems
Issue:
Shutting down the HPLC for a long period requires following this general procedure to prevent damage to the system and the column.
Steps to follow:
Store the...
This Information Applies To: Agilent G7129A/B Autosampler with Sample Thermostat/Cooler G7167-60101 or G7167-60005.
Issue:
The autosampler may stop working from time to time, potentially giving off loud noises and switching off the light. The only...
This Information Applies To: Agilent 5977A/B GC/MSD with EI source, EI Extractor Source, or CI Source.
Issue:
During normal operation of the GC/MSD, the source will require cleaning. It is time to clean the source when:
There is a loss in analyte...
This Information Applies To: Agilent HES source, Agilent 5977 Series GC/MSD
Issue:
During normal operation of the GC/MSD, the source will require cleaning. It is time to clean the source when:
There is a loss in analyte response not improving...
This Information Applies To: Agilent 5977 and 5975 Series GC/MSD systems
Issue
The autotune fails and reports the error Tune action stopped: Gain and offset = 0 and peaks are too narrow!
Resolution
The MSD autotune program is run after routine...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900/8800/8900)
Issue
Condition new or cleaned ICP-MS skimmer cones and sampler cones by aspirating a Conditioning Solution before use.
Background
Drift up can be a sign of...
Turn On the GC/MS Interface and Oven Using OpenLab CDS
Multiple Results
This Information Applies To: Agilent GC/MS instruments controlled by OpenLab CDS software
Issue
Turning on the GC/MS interface heater and Oven using OpenLab CDS software.
Steps to Follow
From the Home tab, click Method > Instrument Setup...
This Information Applies To: Agilent ICP-MS systems (7700/7800/7850/7900)
Issue
The signal monitor function in MassHunter can help with troubleshooting low sensitivity, carry over, contamination, or high background. It can also be used to optimize...
This Information Applies To: Agilent UV detectors (Variable Wavelength Detectors, Multiple Wavelength Detectors, and Diode Array Detectors)
Issue
Checking accumulated hours on the UV lamp.
Steps to Follow
There are four ways to check the accumulated...
This Information Applies To: Agilent 7700/7800/7850/7900/8800/8900 ICP-MS
Issue:
Poor internal standard (ISTD) mixing can cause high relative standard deviation (RSD).
The recommendations in this article are applicable if:
It takes a long...