I am trying to quantitate a radioactive compound. I have the unlabeled standard and it sets up a cal curve very well. However, the synthetic samples suffer from degradation and it generates two other compounds in addition to parent analyte.
So I am trying to use analyte as quantifier, with the two degradants as qualifiers along with the area sum feature.
But when I analyze batch only one of the qualifiers integrates and adds to the calculated concentration. Occasionally, I can use the split peak and pick right to switch from one qualifier to the other but I can only ever get one of the two to integrate and be part of the compound table calculations.
The middle qualifier is the one that will not integrate even though the signal strength is greater.
Thanks for the help