I want to check Total hydrocarbon by FID without identifying the hydrocarbon species . Agilent suggest to give me DB-1 15m, 0.32mm, 0.10u as a non polar column to elute all HC without separation as one peak . Does this column will work for Total hydrocarbon…
Hello,
I am getting the following error on OpenLab CDS Chemstation Edition (Rev. C01.10 [287]): "User Change (Unlock) failed, because instrument access is not permitted for user. Logging Out User". We are initially able to login once, but then when…
Hello mdeighan ,
Manual integration is limited to the rules of the selected integrator and the settings of your quant method. The error and behavior you are seeing typically indicate that the peak you are attempting to create is too far outside of the…
The mass calibration/check for the quadrupole is failing across all isolation widths. Mass delta on 322m/z exceeds limits.
We system tuned a few weeks ago. Can someone please outline the troubleshooting workflow for this type of issue (where to start…
Hi silencer2008,
the 1 µL/s rule means the injection speed used for splitless injections, which is very slow compared to split injection where you want to inject as fast as possible.
Two interesting articles would be:
(+) Pre-Columns - the forgotten…
I am currently having a flow issue with my 6890N GC(w/ G1888 HS). I am doing yearly flow checks. Hooked up a calibrated flow meter to DET exhaust and turned off all gases (pressure off, makeup He off, Air off everything). I then enabled them one at a…
If you receive an onscreen notification to contact Agilent for your service or support request, please do so. Some instruments cannot have service tickets generated through the CrossLab Connect software.
If you receive an email that your service ticket…
Hello, Our lab has a GC-MS (7890B/5977B) system which uses MassHunter version B.07.01 SP1. We recently installed a FID on the system to run FID analysis separate from the MS. We are finding that MassHunter is not as suitable to use for FID analysis in…
Hi joonseok
Put the samples in a separate sequence to the wash runs. In the sequence parameters for the samples, select the post sequence option to switch off the lamps. Run the sample sequence and queue up the wash sequence from the Run control menu…
I have an agilent GC-FID 6890 i use for TPH and PAH of soil samples yet i want to calibrate it for Oxygenates in gasoline and Aromatics don't know how to go about it
This Information Applies To: Agilent OpenLab CDS (version 2.x)
Contents:
In the following procedure, you will find steps to create a multipoint ESTD calibration method with OpenLab CDS 2.X.
Steps to follow:
1. Load the Data
a. From Data...
This Information Applies To: Agilent MassHunter Quantitative Analysis Software
Issue
Chromatographic peak integration is a critical part of accurate and reproducible quantitative data analysis. The integrator type and the integration parameters...
This Information Applies To: Agilent 6200/6400/6500 Series LC/MS Systems
Issue
Instructions on how to fill the calibrant bottle on 6200/6400/6500 Series LC/MS Instruments when calibrant levels are running low.
Background
The ability to autotune...
This Information Applies To: All Agilent 6000 Series LC/MS Systems without a gate valve for ion capillary installation/removal.
Issue:
Installing the Ion Transfer Capillary after cleaning or replacement. For instructions for installing an ion capillary...
This Information Applies To: AriaMx Real-time PCR System
Issue
The saturation level is unique for each optical module after the offset of calibration factor and background calibration. The FAM, ROX, HEX, CY3 & CY5 optical modules will saturate at...
This Information Applies To: Agilent LC Systems
Issue
While it is possible to combine modules from different HPLC series such as 1100, 1200, 1260 or 1290 series to create a functioning LC system, there are some important topics to consider.
...
Fixes for the "RPC Server Unavailable" Error
Multiple Results
This Information Applies To: Agilent OpenLab CDS
Issue
When launching the instrument Acquisition screen/instrument session, there is an "RPC Server Unavailable" error.
Resolution
Accessing the Services App (Windows)
There are two ways to...
This Information Applies To: Agilent LC Pumps
Issue
If a user suspects that the gradient composition isn’t accurate and causes poor chromatography such as retention time shifts, late, early, no peaks or merging peaks. This article provides a quick...
This Information Applies To: Agilent 1290 Infinity (G4226A) and Agilent 1260 Infinity (G1367E) HiP Autosampler
Issue
Replacing the Needle Seat of the Autosampler is required when:
The needle seat is visibly damaged.
Leaks or blockages in the...
This Information Applies To: Agilent OpenLab CDS
Issue
This article discusses different types of bracketing modes and how to set up a bracketed calibration in Data Analysis for OpenLab CDS 2.x
Background
Occasionally, the instrument conditions...