Update: FID output signal was very low even when trying to ignite, so we checked the interconnect spring and noticed it was shorter than the ones in the other GCs (not that close to the detector base; dont know if it was always like that or something…
Hi,
We are struggling to solve an issue with an Agilent 8860 GC-FID we purchased in 2019. It is used to quantify propane in headspace samples that are manually injected. It is possible but unlikely that some of those headspace samplings result in the…
Tip for other users that may encounter an FID Ignition problem: try blowing on the FID when it is trying to light. If the FID lights - there is an issue with the gas flows. It is best to use a flow meter like the ADM Flow Meter for gas chromatography…
Tip for other users that may encounter an FID Ignition problem: try blowing on the FID when it is trying to light. If the FID lights - there is an issue with the gas flows. It is best to use a flow meter like the ADM Flow Meter for gas chromatography…
Hey. Johnson we solved the Problem by removing the igniter Castor with collector nut and the spring locks Info the right place. Another Problem could be the malfunction electrometer.
I have a 5890 GC running ASTM D2887, simulated distillation. It is equipped with a FID and recently we noticed the FID won't light. Flows are good and gases are good. Looking at the setpoint/actual reading, it states it is at the correct temperature …
I completed the inlet leak test and it passed and I also completed the FID jet restriction test and it passed. Yet, when I compare scans on the 8890 the peaks shift more compared to the same injections on my 6890. Does anyone have any thought on this…
Hello DET ,
Sorry for the late response on this.
What sort of spiking do you see usually? What is the output of the FID, in pA?
Are you using any UPS systems, or are the GCs plugged directly into the wall?
This Information Applies To: Agilent Atomic Absorption Spectroscopy Systems (240/280 Series Flame AA and 240/280Z/Zeeman/GTA 120 Graphite Furnace)
Issue:
This article includes recommended maintenance procedures to be performed daily, weekly or annually...
This Information Applies To: Agilent SpectrAA Software, Agilent 240/280 Flame Atomic Absorption Systems, 240/280 Zeeman Graphite Furnace Systems
Issue:
How to Reset Lamp Usage Counters or Add a New Lamp in SpectrAA
Caution : All physical...
This Information Applies To: Agilent GTA 120, Agilent 240Z AA Spectrometer, Agilent 280Z AA Spectrometer, Agilent 240FS/GTA120/PSD120/UltrAA System
Issue:
It is important to align the sample probe of the Programmable Sampler Dispenser (PSD) 120...
This Information Applies To: Agilent Flame AA Systems: e.g., 55B, 240FS, 280FS
Issue:
The Flame AA burner and burner components require regular cleaning to maintain system performance. Components include the burner, nebulizer, and spray chamber...
This Information Applies To: Agilent Flame Atomic Absorption (AA) Spectrometers (50/55/240/280 AA)
Issue:
How to clean a blocked nebulizer of a Flame AA, which may be causing low sensitivity or a sample uptake rate below 5 ml/min.
Steps to follow...
This Information Applies To: Agilent Graphite Furnace Systems (PSD 120/GTA 120/240Z AA/280Z AA)
Issue
Maintenance procedure for replacing the syringe and plunger of the PSD 120 sample dispenser for the Agilent GTA and Zeeman Graphite Furnace Systems...
This Information Applies To: Agilent AA (AA240, AA280) with Graphite Furnace Accessory (GTA)
Issue:
The Programmable Sample Dispenser (PSD) requires the sampling probe to be accurately aligned before the PSD can be used.
The PSD enables the...
This Information Applies To: All Agilent AA systems: 55B, 240FS, 280FS, 240Z, 280Z
Issue:
Optimizing the position of the lamp maximizes amount of light from the lamp passing through the optics to the detector, improving the signal-to-noise and the...
This Information Applies To: Agilent VGA 77, AA, VGA 77P, ICP
Issue:
The Agilent Vapor Generation Accessories VGA 77 and VGA 77P use high concentrations acids. The system needs to be thoroughly cleaned after each use.
The Vapor Generation Accessory...
This Information Applies To: All Agilent Atomic Absorption Spectrometry Systems (AA50, AA55, AA240, AA280)
Issue: This article describes when and how to clean an AA burner.
Background
For optimum and safe performance, burners (see Figure 1 ...