Latest attempt: Curve-- only injected the first two vials then no more but continued the 90 minute acquisition.
This quick test performed all injections-- I believe it worked because the volumes where less than ~20ul. If I adjust injection volumes to greater than 40 or 50ul then it may perform the first three or four injections but never all injections at the higher volumes.
This quick test did not work and I believe it is because the volumes are too large and for some reason it does not like volumes greater than ~20ul. It only performed the first three or four injections.