Is there any specific method or parts to get RSD (<10%) and Linearity from 1ppb to 100ppb (>0.99) in Pesticide standards (including organo-phosphate), 7010B GC/TQ with 7890B GC system.
Is there any specific method or parts to get RSD (<10%) and Linearity from 1ppb to 100ppb (>0.99) in Pesticide standards (including organo-phosphate), 7010B GC/TQ with 7890B GC system.
Are you running in MRM mode? What type of inlet and split or splittless?
Are you running in MRM mode? What type of inlet and split or splittless?
Thank you sir for your prompt response.
I am running with MRM mode and inlet is Pulsed Splitless with 280 temperature. Injection volume is 0.8 microliter.
Have you tried a 50 psi pulse for .5 minutes and purge flow to split vent of 60ml/min at .48 minutes?