I want to determine the concentrations of CO, CO2 and H2 in syngas samples using mass spectrometry as I currently do not have the right GC column for it. Is it possible to do this? Can anyone guide me with the protocol for this? My setup consists of a GC column (HP-5). I will be manually injecting the samples and they have to pass through the column as there is no provision for direct injection into the MS.
