roy_milouot

BFB tune problem (VOC method)

Discussion created by roy_milouot on Sep 15, 2019

Hi all

 

I have recently encountered a problem in my bfb.u tune file parameters..

All of the sudden, my 5973 won't pass bfb tune (*inconsistent peek width*) (pic 1) though it passes Atune (pic 2) just fine..

 

Enclosed for reference are images taken from profile scan in manual tune

 

PIC 1

Atune profile scan

 

PIC 2

Bfb profile scan

 

 

* running MSD chemstation G1701EA E.02.02.1431

 

a few corrective actions I've run through already:

- filament change (both of them)

- column trimming (both ends), septa liner change

- Ion source cleaning (according to Agilent 5973 hardware manual document)

 

** haven't tried MSD baking (don't believe it would help)

 

We believe this bfb tune failure directly effects the following step of the VOC method of BFB P&T injection and running/ passing its test (pic 3)  

 

It keeps failing at the same mass target comparison of 50 to 95... which led us to believe a problem exists with tuning at the lower masses..

 

*** While opening the MS for cleaning we noticed the quad mass filter heater assembly wires (only the two upper white ones) have been welded.. probably an old "fix".. so I am wondering if this could effect low mass selective..? of course, all temperatures are as they should be..

 

Will appreciate any input

Thanks in advance

Roy

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