Column flow/pressure drops during desorb

Hi everyone 

I am new in this platform and i am hoping to learn more. 

I recently removed my column and trimed it but when i replaced it back i have experienced the following: immediately after purge and trap desorbs the column flow drops for the set time of desorption. The tune report has passed. I have change the liner, gold seal, and septum but doesn't help the situation. 

I have been doing this same exercise(trimming) before when i was still using the chemstation software. Now the software is changed to mas hunter and since then we have been experiencing problems. Part of the other problem is that the pulsed plit injection doesnt work anymore. 

Could this dropping of column flow be connected to the software upgrade or it is a hardware problem? And what could it be? 

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  • Yes, probably. But that's with no restrictions on the outlet like the GC inlet, liner, column, column connection, transferline connection, etc.  You can get flow with no outlet back pressure and no flow with it.  What is the carrier supply pressure to the GC and P&T?  The pressure at the transferline outlet must be able to reach at least 63kPa (9.2psi) there.  Any pressure regulation/flow controller needs to be around 140kPa higher than the total of what is downstream of it.  At your final oven temp the inlet is ~164kPa (23.7psi). The trap and plumbing is a restriction, the EPC module, too, so you should have your supply set to at ~482kPa (70psi) or so.  If the gas line filter is plugged up a bit, your trap plugged up a bit, or you have any further restrictions it may required higher pressure than that.

    If this started after you did P&T and column maintenance, I would suggest you go back and do those again to make sure they're as expected. 

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