GCMS with HS

Hi all I need to look at quantifying the content of citronellol (bp 225degC) in a sample via GCMS. The sample is likely to be an oily material that we would not want to directly inject so I was going to take the approach similar to residual solvent headspace analysis - has anyone utilised headspace for quantifying of heavy boiling analytes? any tips or recommendations of application notes to look at? Thank you

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