Hello everyone,
is it Ok to run ICP-OES with a cracked torch ? I face this issue almost every 200 samples or so.
Thanks
Hello everyone,
is it Ok to run ICP-OES with a cracked torch ? I face this issue almost every 200 samples or so.
Thanks
Hi,
i cannot recommend to use a cracked torch at all. In fact, the torch normally should last longer than 200 Samples (if we talk about a normal HNO3 Matrix).
What type of instrument do you have? Maybe the work coil alignment is not perfect.
Best Regards
Chris
Hello Chris
I am using an Agilent 725 ICP-OES, and I'm working with organic matrix (kerosene, mineral oil, veg oils). I noticed a lot suits at the tip of the torch even when injecting O2.
Any thought!
Best,
Hayat
Hello Chris
I am using an Agilent 725 ICP-OES, and I'm working with organic matrix (kerosene, mineral oil, veg oils). I noticed a lot suits at the tip of the torch even when injecting O2.
Any thought!
Best,
Hayat
Normally with an radial instrument (standing torch) there are no problems.
with organic matrix, I guess you are using a conical nebulizer and a torch with a narrow injector.
you could try to increase the plasma gas and aux gas flows
this should help to present torch damages.
Indeed, I am using a radial instrument with the appropriate nebulizer, tubing, and torch for organic matrix.
thanks Chris for your suggestion.
Any thought what is the best internal standard for organic matrix (i.e Y vs. Sc). when I used the Y , it's ratio keep falling down from sample to sample in the same sequence.
sample | Y 360.074 | Sc 255.235 |
blank | 1 | 1 |
2ppm | 0.88 | 1.00 |
5ppm | 0.87 | 1.00 |
10ppm | 0.86 | 0.99 |
blank | 0.89 | 1.04 |
QC | 0.84 | 0.96 |
blank | 0.89 | 1.04 |
oil1 | 0.85 | 0.95 |
blank | 0.88 | 1.04 |
oil2 | 0.83 | 0.93 |
blank | 0.89 | 1.04 |
oil3 | 0.85 | 0.95 |
blank | 0.89 | 1.04 |
oil4 | 0.85 | 0.95 |
blank | 0.89 | 1.05 |
oil4 | 0.84 | 0.97 |
blank | 0.87 | 1.04 |
QC | 0.83 | 0.97 |
Thank you Chris
yes we have radial view, the setup is for organic matrix.
thanks you so much for the suggestion.