INSTRUMENT CONTROL PARAMETERS: GCMS -------------------------------------- Fri May 27 14:00:29 2022 Control Information ------- ----------- Sample Inlet : GC Injection Source : GC ALS Injection Location: Front Mass Spectrometer : Enabled No Sample Prep method has been assigned to this method. GC GC Summary Run Time 16 min Post Run Time 0 min Cycle Time Optimization Fast Cool (default) Oven Temperature Setpoint On (Initial) 70 °C Hold Time 7 min Post Run 70 °C Program #1 Rate 20 °C/min #1 Value 150 °C #1 Hold Time 5 min Equilibration Time 0.25 min Max Temperature 240 °C Maximum Temperature Override Disabled Slow Fan Disabled ALS Injector Syringe Size 10 μL Injection Volume 0.2 μL Solvent A Washes (PreInj) 3 Solvent A Washes (PostInj) 3 Solvent A Volume 4 μL Solvent B Washes (PreInj) 3 Solvent B Washes (PostInj) 3 Solvent B Volume 4 μL Sample Washes 3 Sample Wash Volume 4 μL Sample Pumps 6 Dwell Time (PreInj) 0 min Dwell Time (PostInj) 0 min Solvent Wash Draw Speed 300 μL/min Solvent Wash Dispense Speed 6000 μL/min Sample Wash Draw Speed 300 μL/min Sample Wash Dispense Speed 6000 μL/min Injection Dispense Speed 6000 μL/min Viscosity Delay 0 sec Sample Depth Disabled Injection Type Standard L1 Airgap 0.2 μL Solvent Wash Mode A, B Sample Overlap Mode Sample overlap is not enabled ALS Errors Pause for user interaction SS Inlet He Mode Split Heater On 250 °C Pressure On 2.0699 psi Total Flow On 57 mL/min Septum Purge Flow On 6 mL/min Pre-Run Flow Test On Pre-Run Flow Test Action on Failure Abort Gas Saver Off Split Ratio 50 :1 Split Flow 50 mL/min Liner A Liner has not been selected. Column Column #1 Flow Setpoint On (Initial) 1 mL/min Post Run 0.57353 mL/min Column Information Agilent 123-9334UI-INT: US20400239 DB-BAC1 UI Temperature Range 20 °C—270 °C (270 °C) Dimensions 30 m x 320 μm x 1.8 μm Column lock Locked In SS Inlet He Out MSD (Initial) 70 °C Pressure 2.0699 psi Flow 1 mL/min Average Velocity 30.691 cm/sec Holdup Time 1.6291 min Control Mode Constant Flow Column Outlet Pressure 0 psi Agilent Intuvo 9000 GC Components Guard Chip Temperature Setpoint On (Initial) 210 °C Post Run 100 °C Model Number G4587-60565: Intuvo SSI Guard Chip Track Oven Off Max Temperature 450 °C Isothermal Setpoints Bus Temperature On 200 °C Use Default Bus Temperature On Valve 1 Type Gas Sampling Valve GSV Loop Volume 1 mL Load Time 0.5 min Inject Time 0.5 min Signals Signal #1: Test Plot Description Test Plot Save Off Data Rate 50 Hz Signal #2: Description None Signal #3: Description None Signal #4: Description None MS Information -- ----------- General Information ------- ----------- Acquisition Mode : SIM Solvent Delay (minutes) : 4.5 Tune file : D:\MassHunter\GCMS\1\5977\ATUNE.U EM Setting mode Gain : 5.000000 Number of SIM Groups : 2 Run Time (if MS only) : 650 minutes [SIM Parameters] Group 1 Group ID : toluen Resolution : 0 Group Start Time : 4.5 Number of Ions : 2 Ions Dwell In Group :( Mass, Dwell) ( Mass, Dwell) ( Mass, Dwell) ( 91.00,50 ) ( 92.00,50 ) Group 2 Group ID : amyl alcohol Resolution : 0 Group Start Time : 5.8 Number of Ions : 2 Ions Dwell In Group :( Mass, Dwell) ( Mass, Dwell) ( Mass, Dwell) ( 55.00,50 ) ( 70.00,50 ) [MSZones] MS Source : 230 C maximum 250 C MS Quad : 150 C maximum 200 C Timed Events ----- ------ Number Events= 0 END OF MS ACQUISITION PARAMETERS TUNE PARAMETERS for SN: US1422L218 --------------------------------- Trace Ion Detection is OFF. 34.593 : EMISSION 70.007 : ENERGY 31.712 : REPELLER 90.331 : IONFOCUS 17.627 : ENTRANCE_LENS 1121.040 : EMVOLTS 1388 : Actual EMV 5.00 : GAIN FACTOR 358.000 : AMUGAIN 123.938 : AMUOFFSET 1.000 : FILAMENT 0.000 : DCPOLARITY 15.482 : ENTLENSOFFSET 0.000 : Ion_Body 0.000 : EXTLENS -1040.000 : MASSGAIN -35.000 : MASSOFFSET END OF TUNE PARAMETERS ---------------------- END OF INSTRUMENT CONTROL PARAMETERS ------------------------------------