INSTRUMENT CONTROL PARAMETERS: GCMS#1 ---------------------------------------- C:\MSDCHEM\1\METHODS\ZXH-STEROL-M10-40MIN-MS-1ULIN-SPLITLESS-BACK.M Thu Aug 31 13:15:54 2023 Control Information ------- ----------- Sample Inlet : GC Injection Source : GC ALS Mass Spectrometer : Enabled Oven Equilibration Time 0.5 min Oven Program On 200 蚓 for 1 min then 4 蚓/min to 270 蚓 for 1 min then 1 蚓/min to 290 蚓 for 0.5 min Run Time 40 min Back Injector Syringe Size 10 無 Injection Volume 1 無 Solvent A Washes (PreInj) 2 Solvent A Washes (PostInj) 0 Solvent A Volume 5 無 Solvent B Washes (PreInj) 0 Solvent B Washes (PostInj) 2 Solvent B Volume 5 無 Sample Washes 0 Sample Wash Volume 1 無 Sample Pumps 6 Dwell Time (PreInj) 0 min Dwell Time (PostInj) 0 min Solvent Wash Draw Speed 300 無/min Solvent Wash Dispense Speed 6000 無/min Sample Wash Draw Speed 300 無/min Sample Wash Dispense Speed 6000 無/min Injection Dispense Speed 6000 無/min Viscosity Delay 0 sec Sample Depth Disabled Front SS Inlet He Mode Splitless Heater Off Pressure Off Total Flow Off Septum Purge Flow Off Gas Saver On 20 mL/min After 2 min Purge Flow to Split Vent 50 mL/min at 2 min Back SS Inlet He Mode Splitless Heater On 300 蚓 Pressure On 19.417 psi Total Flow On 19 mL/min Septum Purge Flow On 3 mL/min Gas Saver On 20 mL/min After 2 min Purge Flow to Split Vent 15 mL/min at 0.75 min Thermal Aux 2 {MSD Transfer Line} Heater On Temperature Program On 230 蚓 for 0 min Run Time 40 min Column #1 350 蚓: 30 m x 250 痠 x 0.25 痠 In: Back SS Inlet He Out: Vacuum (Initial) 200 蚓 Pressure 16.089 psi Flow 1 mL/min Average Velocity 38.737 cm/sec Holdup Time 1.2907 min Flow Program Off 1 mL/min for 0 min Run Time 40 min Column #2 350 蚓: 30 m x 250 痠 x 0.25 痠 In: Back SS Inlet He Out: Front Detector FID (Initial) 200 蚓 Pressure 19.417 psi Flow 1 mL/min Average Velocity 30.944 cm/sec Holdup Time 1.6158 min Flow Program Off 1 mL/min for 0 min Run Time 40 min Front Detector FID Heater Off H2 Flow Off Air Flow Off Makeup Flow On 3 mL/min Const Col + Makeup Off Flame Off Electrometer On Signals Test Plot Save Off 50 Hz Test Plot Save Off 50 Hz Test Plot Save Off 50 Hz Test Plot Save Off 50 Hz MS ACQUISITION PARAMETERS General Information ------- ----------- Tune File : atune.u Acquistion Mode : Scan MS Information -- ----------- Solvent Delay : 10.00 min EMV Mode : Gain Factor Gain Factor : 1.00 Resulting EM Voltage : 2165 [Scan Parameters] Low Mass : 50.0 High Mass : 550.0 Threshold : 150 Sample # : 2 A/D Samples 4 Plot 2 low mass : 50.0 Plot 2 high mass : 550.0 [MSZones] MS Source : 230 C maximum 250 C MS Quad : 150 C maximum 200 C END OF MS ACQUISITION PARAMETERS TUNE PARAMETERS for SN: US83140737 ----------------------------- Trace Ion Detection is OFF. EMISSION : 34.610 ENERGY : 69.922 REPELLER : 33.641 IONFOCUS : 90.157 ENTRANCE_LE : 3.000 EMVOLTS : 2188.235 Actual EMV : 2164.71 GAIN FACTOR : 0.99 AMUGAIN : 1604.000 AMUOFFSET : 104.938 FILAMENT : 1.000 DCPOLARITY : 0.000 ENTLENSOFFS : 19.827 MASSGAIN : -767.000 MASSOFFSET : -47.000 END OF TUNE PARAMETERS ------------------------------------ END OF INSTRUMENT CONTROL PARAMETERS ------------------------------------