INSTRUMENT CONTROL PARAMETERS: 1 ----------------------------------- Mon Sep 18 12:19:39 2023 Control Information ------- ----------- Sample Inlet : GC Injection Source : External Device Mass Spectrometer : Enabled Injection Location: Rear No Sample Prep method has been assigned to this method. GC GC Summary Run Time 16.091 min Post Run Time 0 min Oven Temperature Setpoint On (Initial) 36 °C Hold Time 1 min Post Run 70 °C Program #1 Rate 9 °C/min #1 Value 150 °C #1 Hold Time 0 min #2 Rate 33 °C/min #2 Value 230 °C #2 Hold Time 0 min Equilibration Time 0.25 min Max Temperature 230 °C Maximum Temperature Override Disabled Slow Fan Disabled Front SS Inlet He Excluded from Readiness ***Excluded from Affecting GC's Readiness State*** Mode Sleep Heater Off Pressure Off Septum Purge Flow Off Pre-Run Flow Test Off Liner Agilent 5183-4709: 140 μL (Direct, straight (gas samples, HS, P&) Back PTV Inlet He Mode Solvent Vent Pressure On 6.8361 psi Total Flow On 14 mL/min Septum Purge Flow On 3 mL/min Septum Purge Flow Mode Standard Pre-Run Flow Test Off Gas Saver On 20 After 2 min mL/min Purge Flow to Split Vent 10 mL/min at 0.01 min Vent Flow 50 mL/min per min Vent Pressure 6.83 psi Until 0 min Liner Agilent G1544-80730: 675 μL (Direct connect, single taper, bottom ) Column Column #3 Flow Setpoint On (Initial) 1 mL/min Post Run 1.1952 mL/min Column Information Agilent Restek-Rxi5SilMS Temperature Range -60 °C—350 °C (350 °C) Dimensions 30 m x 250 μm x 0.25 μm Column lock Unlocked In Back PTV Inlet He Out MSD (Initial) 36 °C Pressure 6.8361 psi Flow 1 mL/min Average Velocity 36.187 cm/sec Holdup Time 1.3817 min Control Mode Constant Flow Column Outlet Pressure 0 psi Front Detector FID Excluded from Readiness ***Excluded from Affecting GC's Readiness State*** Makeup He Heater On 275 °C H2 Flow Off Air Flow Off Makeup Flow Off Carrier Gas Flow Correction Constant Makeup and Fuel Flow Flame Off Detector Evaluation Perform Detector Evaluation Test Off Signal Selected No Signal Selected Checkout Sample None MSD Transfer Line Temperature Setpoint On (Initial) 280 °C Aux EPC 1,2,3 Aux EPC 1 N2 Pressure Setpoint Off (Initial) 10 psi Post Run 10 psi Excluded from Readiness ***Excluded from Affecting GC's Readiness State*** Aux EPC 2 N2 Pressure Setpoint Off (Initial) 10 psi Post Run 10 psi Excluded from Readiness ***Excluded from Affecting GC's Readiness State*** Aux EPC 3 N2 Pressure Setpoint Off (Initial) 10 psi Post Run 10 psi Excluded from Readiness ***Excluded from Affecting GC's Readiness State*** PSD 2 Pressure Setpoint Off (Initial) 10 psi Post Run 10 psi Excluded from Readiness ***Excluded from Affecting GC's Readiness State*** PSD Purge Off Signals Signal #1: Description None Signal #2: Description None Signal #3: Description None Signal #4: Description None Signal #5: Description None Signal #6: Description None Signal #7: Description None Signal #8: Description None GERSTEL MAESTRO SYSTEM SETTINGS Maestro Runtime : 16.09 min GC Cool Down Time : 5.00 min Cryo Timeout : 15.00 min GERSTEL CIS CIS : used CRYO COOLING Cryo Cooling : used TEMPERATURE PROGRAM Heater Mode : Standard Liner Type : 013882-010-00 glass liner CIS4, baffled, non deactivated Liner Max Temperature : 400 'C Initial Temperature : -10 'C Equilibration Time : 0.50 min Initial Time : 0.50 min Ramp 1 Rate : 12.00 'C/s End Temp : 325 'C Hold Time : 5.00 min Ramp 2 Rate : 0.0 'C/s Low Split : not used GERSTEL TDU TEMPERATURE PROGRAM Initial Temperature : 40 'C Delay Time : 0.50 min Initial Time : 0.50 min Ramp 1 Rate 1 : 720.0 'C/min End Temp 1 : 320 'C Hold Time 1 : 7.00 min Ramp 2 Rate 2 : 0.0 'C/min TDU SETTINGS Transfer Temp : 280 'C Transfer Temp Mode : Fixed Desorption Mode : Splitless Sample Mode : Remove Tube - Standby Cooling Standby Temp : 40 'C TDU LIQUID OPTION Liquid Option : not used - use these parameters if it becomes 'used' Sample Tray : Rack 1,VT54/2-CVM Fixed Liquid Vial : used Liquid Vial : 1 Inject into Micro vial : not used PYROLYSIS PARAMETERS Pyrolysis : not used - use these parameters if it becomes 'used' Pyro Mode : Pyro in last hold (standard) Pyrolysis Lead Time : 0.10 min Pyrolysis Followup Time : 1.00 min Pyrolysis Initial Time : 0.50 min Pyrolysis Initial Temp. : 500 'C Pyrolysis Rate 1 : 0.00 'C/s Pyrolysis Rate 2 : 0.00 'C/s Pyrolysis Heater : used GERSTEL DHS DHS : not used - use these parameters if it becomes 'used' DHS Module : DHS INJECTION TUBE Tube Tray : TDUTray1,VT40t/Tube Fixed Tube : used Tube Number : 1 PURGE TUBE Purge Tube : not used - use these parameters if it becomes 'used' Purge Tube Tray : Tube Number : INCUBATION SETTINGS Incubation Temperature : 30 'C Incubation Time : 1.00 min AGITATION SETTINGS Agitator On Time : 60 s Agitator Off Time : 1 s Agitator Speed : 500 rpm TRANSFER HEATER SETTINGS TEMP : 75 'C PURGE PHASE SETTINGS Volume : 0.0 mL TRAPPING PHASE SETTINGS Volume : 50.0 mL Flow : 20.0 mL/min Trap Temperature : 25 'C Incubation Temperature : 30 'C DRYING PHASE SETTINGS Volume : 0.0 mL MS Information -- ----------- General Information ------- ----------- Acquisition Mode : SIM/Scan Solvent Delay (minutes) : 1 Tune file : D:\MassHunter\GCMS\1\5977\etune.u EM Setting mode Gain : 1.000000 Number of SIM Groups : 3 Run Time (if MS only) : 16 minutes [Scan Parameters] Start Time : 1 Low Mass : 35 High Mass : 350 Threshold : 100 A/D Samples: : 8 [SIM Parameters] Group 1 Group ID : Null Resolution : 0 Group Start Time : 1 Number of Ions : 1 Ions Dwell In Group :( Mass, Dwell) ( Mass, Dwell) ( Mass, Dwell) ( 450.00,50 ) Group 2 Group ID : MMA Resolution : 0 Group Start Time : 3.52 Number of Ions : 5 Ions Dwell In Group :( Mass, Dwell) ( Mass, Dwell) ( Mass, Dwell) ( 41.00,50 ) ( 69.00,50 ) ( 85.00,50 ) ( 99.00,50 ) ( 100.00,50 ) Group 3 Group ID : Null Resolution : 0 Group Start Time : 3.9 Number of Ions : 1 Ions Dwell In Group :( Mass, Dwell) ( Mass, Dwell) ( Mass, Dwell) ( 450.00,50 ) [MSZones] MS Source : 230 C maximum 250 C MS Quad : 150 C maximum 200 C Timed Events ----- ------ Number Events= 0 END OF MS ACQUISITION PARAMETERS TUNE PARAMETERS for SN: US2018M021 --------------------------------- Trace Ion Detection is OFF. 34.593 : EMISSION 70.007 : ENERGY 0.503 : REPELLER 88.835 : IONFOCUS 12.582 : ENTRANCE_LENS 1509.614 : EMVOLTS 1752.4 : Actual EMV 1.00 : GAIN FACTOR 1869.000 : AMUGAIN 140.125 : AMUOFFSET 1.000 : FILAMENT 0.000 : DCPOLARITY 11.650 : ENTLENSOFFSET 10.002 : Ion_Body -2.800 : EXTLENS -244.000 : MASSGAIN -28.000 : MASSOFFSET END OF TUNE PARAMETERS ---------------------- END OF INSTRUMENT CONTROL PARAMETERS ------------------------------------