INSTRUMENT CONTROL PARAMETERS: GCMSD --------------------------------------- Mon Jul 08 13:06:39 2024 Control Information ------- ----------- Sample Inlet : GC Injection Source : External Device Mass Spectrometer : Enabled No Sample Prep method has been assigned to this method. ============================================================================= 6890 GC METHOD ============================================================================= OVEN Initial temp: 35 'C (On) Maximum temp: 325 'C Initial time: 4.00 min Equilibration time: 1.50 min Ramps: # Rate Final temp Final time 1 10.00 230 1.50 2 0.0(Off) Post temp: 0 'C Post time: 0.00 min Run time: 25.00 min FRONT INLET (SPLIT/SPLITLESS) BACK INLET (UNKNOWN) Mode: Split Initial temp: 250 'C (On) Pressure: 6.77 psi (On) Split ratio: 5:1 Split flow: 5.0 mL/min Total flow: 8.6 mL/min Gas saver: Off Gas type: Helium COLUMN 1 COLUMN 2 Capillary Column (not installed) Model Number: Agilent 19091S-433 HP-5MS 5% Phenyl Methyl Siloxane Max temperature: 325 'C Nominal length: 30.0 m Nominal diameter: 250.00 um Nominal film thickness: 0.25 um Mode: constant flow Initial flow: 1.0 mL/min Nominal init pressure: 6.78 psi Average velocity: 36 cm/sec Inlet: Front Inlet Outlet: MSD Outlet pressure: vacuum FRONT DETECTOR (NO DET) BACK DETECTOR (NO DET) SIGNAL 1 SIGNAL 2 Data rate: 20 Hz Data rate: 20 Hz Type: test plot Type: test plot Save Data: Off Save Data: Off Zero: 0.0 (Off) Zero: 0.0 (Off) Range: 0 Range: 0 Fast Peaks: Off Fast Peaks: Off Attenuation: 0 Attenuation: 0 COLUMN COMP 1 COLUMN COMP 2 (No Detectors Installed) (No Detectors Installed) THERMAL AUX 2 Use: MSD Transfer Line Heater Description: Initial temp: 280 'C (On) Initial time: 0.00 min # Rate Final temp Final time 1 0.0(Off) POST RUN Post Time: 0.00 min TIME TABLE Time Specifier Parameter & Setpoint GC Injector Front Injector: Injector not configured, use these parameters if it becomes configured Sample Washes 0 Sample Pumps 6 Injection Volume 1.00 microliters Syringe Size 10.0 microliters PostInj Solvent A Washes 0 PostInj Solvent B Washes 0 Viscosity Delay 0 seconds Plunger Speed Fast Back Injector: No parameters specified Column 1 Inventory Number : 19091S-433 Column 2 Inventory Number : MS ACQUISITION PARAMETERS General Information ------- ----------- Tune File : atune.u Acquistion Mode : SIM MS Information -- ----------- Solvent Delay : 1.20 min EMV Mode : Gain Factor Gain Factor : 1.00 Resulting EM Voltage : 1424 [Sim Parameters] GROUP 1 Group ID : 1 Resolution : Low Plot 1 Ion : 62.00 Ions/Dwell In Group ( Mass, Dwell) ( Mass, Dwell) ( 62.00, 100) ( 64.00, 100) GROUP 2 Group ID : 2 Resolution : Low Group Start Time : 1.56 Plot 1 Ion : 53.00 Ions/Dwell In Group ( Mass, Dwell) ( Mass, Dwell) ( Mass, Dwell) ( 51.00, 100) ( 52.00, 100) ( 53.00, 100) GROUP 3 Group ID : 3 Resolution : Low Group Start Time : 2.50 Plot 1 Ion : 70.00 Ions/Dwell In Group ( Mass, Dwell) ( Mass, Dwell) ( 70.00, 100) ( 96.00, 100) GROUP 4 Group ID : 4 Resolution : Low Group Start Time : 5.00 Plot 1 Ion : 117.00 Ions/Dwell In Group ( Mass, Dwell) ( Mass, Dwell) ( 82.00, 100) (117.00, 100) GROUP 5 Group ID : 5 Resolution : Low Group Start Time : 7.00 Plot 1 Ion : 173.00 Ions/Dwell In Group ( Mass, Dwell) ( Mass, Dwell) ( Mass, Dwell) (171.00, 100) (173.00, 100) (175.00, 100) (254.00, 100) GROUP 6 Group ID : 7 Resolution : Low Group Start Time : 9.00 Plot 1 Ion : 152.00 Ions/Dwell In Group ( Mass, Dwell) ( Mass, Dwell) ( Mass, Dwell) (115.00, 100) (150.00, 100) (152.00, 100) [MSZones] MS Source : 230 C maximum 250 C MS Quad : 150 C maximum 200 C Timed Events ----- ------ [Timed MS Detector Table Entries] Time (min) State (MS On/Off) 15.00 Off END OF MS ACQUISITION PARAMETERS TUNE PARAMETERS for SN: US60522243 ----------------------------- Trace Ion Detection is OFF. EMISSION : 34.610 ENERGY : 69.922 REPELLER : 26.940 IONFOCUS : 90.157 ENTRANCE_LE : 32.000 EMVOLTS : 1270.588 Actual EMV : 1423.53 GAIN FACTOR : 1.02 AMUGAIN : 1619.000 AMUOFFSET : 123.375 FILAMENT : 1.000 DCPOLARITY : 0.000 ENTLENSOFFS : 17.569 MASSGAIN : -680.000 MASSOFFSET : -33.000 END OF TUNE PARAMETERS ------------------------------------ END OF INSTRUMENT CONTROL PARAMETERS ------------------------------------