INSTRUMENT CONTROL PARAMETERS:    GCQQQ-2
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   D:\MassHunter\GCMS\1\methods\EC PBDE\Validation\20240422 PBDE dMRM.M
      Mon Jul 29 11:47:00 2024

Control Information
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Sample Inlet             : GC
Injection Source         : GC ALS
Injection Location:  Front
Mass Spectrometer        : Enabled


 No Sample Prep method has been assigned to this method.


GC
GC Summary
Run Time                                     14.417 min
Post Run Time                                0 min

Oven
Temperature
Setpoint                                     On
(Initial)                                    80 °C
Hold Time                                    1 min
Post Run                                     340 °C
Program
#1 Rate                                      40 °C/min
#1 Value                                     230 °C
#1 Hold Time                                 3 min
#2 Rate                                      30 °C/min
#2 Value                                     325 °C
#2 Hold Time                                 3.5 min


Equilibration Time                           0.5 min
Max Temperature                              350 °C
Maximum Temperature Override                 Disabled
Slow Fan                                     Disabled

ALS
Front Injector
Syringe Size                                 10 μL
Injection Volume                             2 μL
Solvent A Washes (PreInj)                    0
Solvent A Washes (PostInj)                   5
Solvent A Volume                             8 μL
Solvent B Washes (PreInj)                    1
Solvent B Washes (PostInj)                   5
Solvent B Volume                             8 μL
Sample Washes                                0
Sample Wash Volume                           1 μL
Sample Pumps                                 2
Dwell Time (PreInj)                          0 min
Dwell Time (PostInj)                         0 min
Solvent Wash Draw Speed                      300 μL/min
Solvent Wash Dispense Speed                  3000 μL/min
Sample Wash Draw Speed                       300 μL/min
Sample Wash Dispense Speed                   3000 μL/min
Injection Dispense Speed                     6000 μL/min
Viscosity Delay                              2 sec
Sample Depth                                 Disabled
Injection Type                               Standard
L1 Airgap                                    0.2 μL
Solvent Wash Mode                            A, B

Sample Overlap
Mode                                         Sample overlap is not enabled

ALS Errors                                   Pause for user interaction

Front MM Inlet He
Front MM Inlet He Temperature
Setpoint                                     On
(Initial)                                    100 °C
Hold Time                                    0.2 min
Program
#1 Rate                                      900 °C/min
#1 Value                                     330 °C
#1 Hold Time                                 3 min


Mode                                         Pulsed Splitless
Pressure                                     On    15.407 psi
Total Flow                                   On    54 mL/min
Septum Purge Flow                            On    3 mL/min
Septum Purge Flow Mode                       Switched
Pre-Run Flow Test                            Off
Gas Saver                                    On    15 mL/min after 3 min
Injection Pulse Pressure                     50 psi Until 1.5 min
Purge Flow to Split Vent                     50 mL/min at 2.5 min
Cryo                                         On
Cryo Type                                    N2
Fast Cooldown                                On
Cryo Use Temperature                         125 °C
Timeout Detection                            On    10 min
Fault Detection                              On
Liner                                        Agilent 5190-4006: 200 μL (Splitless, dimpled, Ultra Inert)

Back SS Inlet He
Mode                                         Split
Heater                                       Off
Pressure                                     Off
Total Flow                                   Off
Septum Purge Flow                            Off
Pre-Run Flow Test                            Off
Liner                                        A Liner has not been selected.

Column
Column #1
Flow
Setpoint                                     On
(Initial)                                    1 mL/min
Post Run                                     1.2 mL/min

Column Information                           Agilent 19091A-008: ECU01
Description                                  Ultra 1
Temperature Range                            -60 °C—325 °C (350 °C)
Dimensions                                   17 m x 200 μm x 0.11 μm (Uncalibrated)
Main Segment Heated By                       Oven
Segment inSeg                                Heated By Oven: 1.5 m x 180 μm x 0 μm
Column lock                                  Unlocked
In                                           Front MM Inlet He
Out                                          MSD 
(Initial)                                    80 °C
Pressure                                     15.407 psi
Flow                                         1 mL/min
Average Velocity                             48.102 cm/sec
Holdup Time                                  0.641 min
Control Mode                                 Constant Flow

Column Outlet Pressure                       0 psi

Detector Evaluation
Perform Detector Evaluation Test             Off
Signal Selected                              No Signal Selected
Checkout Sample                              None

MSD Transfer Line
Temperature
Setpoint                                     On
(Initial)                                    325 °C


Collision Cell/Aux
Pressure
Setpoint                                     Off
(Initial)                                    10 psi
Post Run                                     10 psi

Quench Gas He                                On    4 mL/min
Collision Gas N2                             On    1.5 mL/min

PSD 1
Pressure
Setpoint                                     Off
(Initial)                                    3.2897 psi
Post Run                                     50 psi

PSD Purge                                    Off

Signals
Signal #1: 
Description                                  None

Signal #2: 
Description                                  None

Signal #3: 
Description                                  None

Signal #4: 
Description                                  None

Signal #5: 
Description                                  None

Signal #6: 
Description                                  None

Signal #7: 
Description                                  None

Signal #8: 
Description                                  None






                      END OF INSTRUMENT CONTROL PARAMETERS
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