INSTRUMENT CONTROL PARAMETERS: Havok --------------------------------------- D:\MassHunter\GCMS\1\methods\METH_QUANT2.M Tue Sep 19 14:51:19 2023 Control Information ------- ----------- Sample Inlet : GC Injection Source : GC ALS Injection Location: Front Mass Spectrometer : Enabled No Sample Prep method has been assigned to this method. GC GC Summary Run Time 4 min Post Run Time 0 min Oven Temperature Setpoint On (Initial) 150 °C Hold Time 0.5 min Post Run 0 °C Program #1 Rate 25 °C/min #1 Value 220 °C #1 Hold Time 0.7 min Equilibration Time 0.5 min Max Temperature 325 °C Maximum Temperature Override Disabled Slow Fan Disabled ALS Front Injector Syringe Size 5 μL Injection Volume 0.5 μL Solvent A Washes (PreInj) 1 Solvent A Washes (PostInj) 3 Solvent A Volume 4 μL Solvent B Washes (PreInj) 1 Solvent B Washes (PostInj) 3 Solvent B Volume 4 μL Sample Washes 1 Sample Wash Volume 4 μL Sample Pumps 3 Dwell Time (PreInj) 0 min Dwell Time (PostInj) 0 min Solvent Wash Draw Speed 150 μL/min Solvent Wash Dispense Speed 1000 μL/min Sample Wash Draw Speed 150 μL/min Sample Wash Dispense Speed 1000 μL/min Injection Dispense Speed 3000 μL/min Viscosity Delay 1 sec Sample Depth 0 mm Injection Type Standard L1 Airgap 0.1 μL Solvent Wash Mode A, B Sample Overlap Mode Sample overlap is not enabled ALS Errors Pause for user interaction Front SS Inlet He Mode Split Heater On 250 °C Pressure On 16.008 psi Total Flow On 1249.8 mL/min Septum Purge Flow On 3 mL/min Pre-Run Flow Test Off Gas Saver On 15 mL/min after 0.5 min Split Ratio 1038 :1 Split Flow 1245.6 mL/min Liner A Liner has not been selected. Column Column #1 Flow Setpoint On (Initial) 1.2 mL/min Post Run 0.57353 mL/min Column Information Agilent 13323-1628655 Description Rxi-1ms Temperature Range -60 °C—325 °C (350 °C) Dimensions 30 m x 250 μm x 0.25 μm (Uncalibrated) Heater Oven Column lock Unlocked In Front SS Inlet He Out MSD (Initial) 150 °C Pressure 16.008 psi Flow 1.2 mL/min Average Velocity 41.683 cm/sec Holdup Time 1.1995 min Control Mode Constant Flow Column Outlet Pressure 0 psi Detector Evaluation Perform Detector Evaluation Test Off MSD Transfer Line Temperature Setpoint On (Initial) 260 °C Signals Signal #1: Description None Signal #2: Description None Signal #3: Description None Signal #4: Description None Signal #5: Description None Signal #6: Description None Signal #7: Description None Signal #8: Description None MS Information -- ----------- General Information ------- ----------- Acquisition Mode : SIM Solvent Delay (minutes) : 1.5 Tune file : D:\MassHunter\GCMS\1\5977\etune.u EM Setting mode Delta : 0.000000 Number of SIM Groups : 1 Run Time (if MS only) : 10 minutes [SIM Parameters] Group 1 Group ID : 1 Resolution : 1 Group Start Time : 1.5 Number of Ions : 4 Ions Dwell In Group :( Mass, Dwell) ( Mass, Dwell) ( Mass, Dwell) ( 58.00,50 ) ( 91.00,50 ) ( 168.00,50 ) ( 169.00,50 ) [MSZones] MS Source : 230 C maximum 250 C MS Quad : 150 C maximum 200 C Timed Events ----- ------ Number Events= 0 END OF MS ACQUISITION PARAMETERS TUNE PARAMETERS for SN: US2312MA29 --------------------------------- Trace Ion Detection is OFF. 34.593 : EMISSION 70.007 : ENERGY 0.503 : REPELLER 89.822 : IONFOCUS 27.717 : ENTRANCE_LENS 928.951 : EMVOLTS 929 : Actual EMV 0.18 : GAIN FACTOR 1640.000 : AMUGAIN 133.938 : AMUOFFSET 1.000 : FILAMENT 0.000 : DCPOLARITY 6.495 : ENTLENSOFFSET 10.002 : Ion_Body 0.303 : EXTLENS -470.000 : MASSGAIN -23.000 : MASSOFFSET END OF TUNE PARAMETERS ---------------------- END OF INSTRUMENT CONTROL PARAMETERS ------------------------------------