INSTRUMENT CONTROL PARAMETERS: 1 ----------------------------------- Thu Oct 26 09:09:01 2023 Control Information ------- ----------- Sample Inlet : GC Injection Source : Manual Mass Spectrometer : Enabled Injection Location: Front No Sample Prep method has been assigned to this method. GC GC Summary Run Time 23.667 min Post Run Time 0 min Oven Temperature Setpoint On (Initial) 36 °C Hold Time 1 min Post Run 70 °C Program #1 Rate 3 °C/min #1 Value 70 °C #1 Hold Time 0 min #2 Rate 30 °C/min #2 Value 320 °C #2 Hold Time 3 min Equilibration Time 0.25 min Max Temperature 350 °C Maximum Temperature Override Disabled Slow Fan Disabled Front SS Inlet He Excluded from Readiness ***Excluded from Affecting GC's Readiness State*** Mode Split Heater On 250 °C Pressure On 6.8361 psi Total Flow On 204 mL/min Septum Purge Flow On 3 mL/min Pre-Run Flow Test Off Gas Saver Off Split Ratio 200 :1 Split Flow 200 mL/min Liner Agilent 5183-4709: 140 μL (Direct, straight (gas samples, HS, P&) Back PTV Inlet He Mode Sleep Pressure Off Septum Purge Flow Off Pre-Run Flow Test Off Liner Agilent G1544-80730: 675 μL (Direct connect, single taper, bottom ) Column Column #3 Flow Setpoint On (Initial) 1 mL/min Post Run 1.1952 mL/min Column Information Agilent Restek-Rxi5SilMS Temperature Range -60 °C—350 °C (350 °C) Dimensions 30 m x 250 μm x 0.25 μm Column lock Unlocked In Front SS Inlet He Out MSD (Initial) 36 °C Pressure 6.8361 psi Flow 1 mL/min Average Velocity 36.187 cm/sec Holdup Time 1.3817 min Control Mode Constant Flow Column Outlet Pressure 0 psi Front Detector FID Excluded from Readiness ***Excluded from Affecting GC's Readiness State*** Makeup He Heater On 300 °C H2 Flow Off Air Flow Off Makeup Flow Off Carrier Gas Flow Correction Constant Makeup and Fuel Flow Flame Off Detector Evaluation Perform Detector Evaluation Test Off Signal Selected No Signal Selected Checkout Sample None MSD Transfer Line Temperature Setpoint On (Initial) 280 °C Aux EPC 1,2,3 Aux EPC 1 N2 Pressure Setpoint Off (Initial) 10 psi Post Run 10 psi Excluded from Readiness ***Excluded from Affecting GC's Readiness State*** Aux EPC 2 N2 Pressure Setpoint Off (Initial) 10 psi Post Run 10 psi Excluded from Readiness ***Excluded from Affecting GC's Readiness State*** Aux EPC 3 N2 Pressure Setpoint Off (Initial) 10 psi Post Run 10 psi Excluded from Readiness ***Excluded from Affecting GC's Readiness State*** PSD 2 Pressure Setpoint Off (Initial) 10 psi Post Run 10 psi Excluded from Readiness ***Excluded from Affecting GC's Readiness State*** PSD Purge Off Signals Signal #1: Description None Signal #2: Description None Signal #3: Description None Signal #4: Description None Signal #5: Description None Signal #6: Description None Signal #7: Description None Signal #8: Description None GERSTEL MAESTRO SYSTEM SETTINGS Maestro Runtime : 23.67 min GC Cool Down Time : 5.00 min Cryo Timeout : 15.00 min GERSTEL CIS CIS : not used - use these parameters if it becomes 'used' CRYO COOLING Cryo Cooling : used TEMPERATURE PROGRAM Heater Mode : Standard Liner Type : 013882-010-00 glass liner CIS4, baffled, non deactivated Liner Max Temperature : 400 'C Initial Temperature : -10 'C Equilibration Time : 0.50 min Initial Time : 0.50 min Ramp 1 Rate : 12.00 'C/s End Temp : 325 'C Hold Time : 5.00 min Ramp 2 Rate : 0.0 'C/s Low Split : not used MS Information -- ----------- General Information ------- ----------- Acquisition Mode : SIM/Scan Solvent Delay (minutes) : 1 Tune file : D:\MassHunter\GCMS\1\5977\etune.u EM Setting mode Gain : 1.000000 Number of SIM Groups : 3 Run Time (if MS only) : 23.6666666666667 minutes [Scan Parameters] Start Time : 1 Low Mass : 60 High Mass : 350 Threshold : 100 A/D Samples: : 8 [SIM Parameters] Group 1 Group ID : Null Resolution : 0 Group Start Time : 1 Number of Ions : 1 Ions Dwell In Group :( Mass, Dwell) ( Mass, Dwell) ( Mass, Dwell) ( 450.00,50 ) Group 2 Group ID : MMA Resolution : 0 Group Start Time : 3.3 Number of Ions : 5 Ions Dwell In Group :( Mass, Dwell) ( Mass, Dwell) ( Mass, Dwell) ( 41.00,50 ) ( 69.00,50 ) ( 85.00,50 ) ( 99.00,50 ) ( 100.00,50 ) Group 3 Group ID : Null Resolution : 0 Group Start Time : 3.8 Number of Ions : 1 Ions Dwell In Group :( Mass, Dwell) ( Mass, Dwell) ( Mass, Dwell) ( 450.00,50 ) [MSZones] MS Source : 230 C maximum 250 C MS Quad : 150 C maximum 200 C Timed Events ----- ------ Number Events= 0 END OF MS ACQUISITION PARAMETERS TUNE PARAMETERS for SN: US2018M021 --------------------------------- Trace Ion Detection is OFF. 34.593 : EMISSION 70.007 : ENERGY 1.399 : REPELLER 89.822 : IONFOCUS 12.582 : ENTRANCE_LENS 1637.429 : EMVOLTS 1784.3 : Actual EMV 1.00 : GAIN FACTOR 1874.000 : AMUGAIN 121.125 : AMUOFFSET 1.000 : FILAMENT 0.000 : DCPOLARITY 7.494 : ENTLENSOFFSET 9.002 : Ion_Body 1.204 : EXTLENS -238.000 : MASSGAIN -35.000 : MASSOFFSET END OF TUNE PARAMETERS ---------------------- END OF INSTRUMENT CONTROL PARAMETERS ------------------------------------